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This study reports flexible nanocomposite-based piezoelectric nanogenerators (PENGs) fabricated by dispersing various piezoelectric nanoparticles (BaTiO3, ZnO, and PZT) and graphene nanopowder in a silicone matrix. The results indicated that the PZT-based composites showed superior performance in comparison to other ceramics. Subsequently, practical application of PENGs was demonstrated by developing a fully functioning shoe-insole nanogenerator (SING). The SING generated high open-circuit voltage (∼27 V), short-circuit current (429.23 μA), and power density (402 mW/m2) under real-time human walking. Moreover, a facile and inexpensive fabrication method for efficient, skin-friendly, and highly stretchable biomechanical piezoelectric sensors is also proposed. In this regard, multiwall carbon nanotubes/silicone composite stretchable electrodes were prepared to be compatible with the sensors. The electrodes displayed stability even under high uniaxial elongation (100%), and the fabricated sensors responded effectively to almost every joint movement. The results suggested that the fabricated PENGs can be potentially used as self-powered biomechanical energy harvesters/sensors in wearable electronics, haptic sensing, or internet of human-related applications.

Blast furnace slag, an industrial by-product, is emerging as a potential raw material to synthesize hydroxyapatite and zeolite. In this study, the effects of temperature on the hydrothermal synthesis of hydroxyapatite-zeolite from blast furnace slag were investigated. Specimens were synthesized at different temperatures (room temperature, 50, 90, 120, or 150 °C). The synthesized specimens were analyzed qualitatively and quantitatively via X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), BET/BJH, and scanning electron microscopy/energy dispersive using X-ray analysis (SEM/EDX). It was found that the hydroxyapatite phase was synthesized at all the reaction temperatures, while faujasite type zeolite appeared in the specimens synthesized at 90 and 120 °C. Moreover, faujasite was replaced by hydroxysodalite in the specimens synthesized at 150 °C. Additionally, the crystals of the hydroxyapatite tended to become larger and total crystallinity increased as the reaction temperature increased.

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