In this paper we have investigated the effects of sintering time and temperature on the formation and critical current densities of Fe-clad MgB2 wires. MgB2 wires were fabricated using the powder-in-tube process and sintered for different periods of time at predetermined temperatures. All the samples were examined using XRD, SEM and magnetisation measurements. In contrast to the common practice of sintering for several hours, the present results show that there is no need for prolonged heat treatment in the fabrication of Fe-clad MgB2 wires. A total time in the furnace of several minutes is more than enough to form nearly pure MgB2 with high performance characteristics. The results from Tc, Jc and Hirr show convincingly that the samples which were sintered for 3 minutes above 800 oC are as good as those sintered for longer times. In fact, the Jc field performance for the most rapidly sintered sample is slightly better than for all other samples. Jc of 4.5 times 10 ^5 A/cm2 in zero field and above 10 ^5 A/cm2 in 2T at 15 K has been achieved for the best Fe-clad MgB2 wires. As a result of such a short sintering there is no need for using high purity argon protection and it is possible to carry out the heat treatment in a much less protective atmosphere or in air. These findings substantially simplify the fabrication process, making it possible to have a continuous process for fabrication and reducing the costs for large-scale production of MgB2 wires.Comment: 15 pages, one table, 9 figures, submitted to Physica C on June 8, 200

In this letter, we report the results of field (H) and temperature (T) dependent magnetization (M) measurements of a pellet of uniform, large-grain sintered MgB 2 . We show that at low temperatures the size of the pellet and its critical current density, J c (H) --i.e. its M(H) --ensure low field flux jumping, which of course ceases when M(H) drops below a critical value. With further increase of H and T the individual grains decouple and the M(H) loops drop to lower lying branches, unresolved in the usual full M(H) representation. After taking into account the sample size and grain size, respectively, the bulk sample and the grains were deduced to exhibit the same magnetically determined J c s (e.g. 10 5 A/cm 2 , 20 K, 0T) and hence that for each temperature of measurement J c (H) decreased monotonically with H over the entire field range, except for a gap within the grain-decoupling zone.

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The fabrication, characterisation, and superconductivity of MgB 2 thick films grown on stainless steel substrate were studied. XRD, SEM, and magnetic measurements were carried out. It was found that the MgB 2 thick films can be fast formed by heating samples to 660 o C then immediately cooling down to room temperature. XRD shows above 90% MgB 2 phase and less than 10 % MgO. However, the samples sintered at 800 o C for 4 h contain both MgB 4 and MgO impurities in addition to MgB 2 . The fast formed MgB 2 films appear to have a good grain connectivity that gives a J c of 8 x 10 4 A/cm 2 at 5 K and 1 T and maintained this value at 20 K in zero field.2

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