The first organic-inorganic hybrid vanadoniobate cluster compounds with a bicapped Keggin-type {VNb(12)O(40)(VO)(2)} core have been synthesized and characterized.
A novel {V(4)Nb(6)O(30)} addenda: Through the successful introduction of a vanadium atom into the polyoxoniobate system, three novel compounds containing the same unprecedented mixed addenda vanadoniobate cluster {V(4)Nb(6)O(30)} were obtained. The incorporation of suitable atoms like V is an intriguing subject providing vast possibilities to enrich polyoxoniobate chemistry.
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