In this work we demonstrate comprehensive studies on graphene oxide (GO) and reduced graphene oxide (rGO) based saturable absorbers (SA) for mode-locking of Er-doped fiber lasers. The paper describes the fabrication process of both saturable absorbers and detailed comparison of their parameters. Our results show, that there is no significant difference in the laser performance between the investigated SA. Both provided stable, mode-locked operation with sub-400 fs soliton pulses and more than 9 nm optical bandwidth at 1560 nm center wavelength. It has been shown that GO might be successfully used as an efficient SA without the need of its reduction to rGO. Taking into account simpler manufacturing technology and the possibility of mass production, GO seems to be a good candidate as a cost-effective material for saturable absorbers for Er-doped fiber lasers.

Low-dimensional materials, due to their versatile properties are very interesting for numerous electronics and optoelectronics applications. Recently rediscovered black phosphorus, with a graphite-like structure can be exfoliated up to the single atomic layer. In contrary to graphene it possesses a direct band gap controllable by the number of stacked atomic layers. For those reasons, it is now intensively investigated. Here we demonstrate, that black phosphorus can serve as a broadband saturable absorber and can be used for ultrashort optical pulse generation.The mechanically exfoliated ~300 nm thick layers of black phosphorus were transferred onto the fiber core and under pulsed excitation at 1560 nm wavelength its transmission increases by 4.4%.It was used to generate 272 fs-short pulses at 1550 nm and 739 fs at 1910 nm. The obtained results shows that black phosphorus can be effectively used for ultrashort pulse generation and proves its great potential to future applications.

We report, for the first time to our knowledge, the usage of black phosphorus (BP) as a saturable absorber for the mode locking of a thulium-doped fiber laser. We have experimentally shown that BP exhibits saturable absorption in the 2 μm wavelength range and supports ultrashort pulse generation. The saturable absorber was based on mechanically exfoliated BP deposited on a fiber connector tip. The laser was capable of generating 739 fs pulses centered at 1910 nm. Our results show that BP might be considered as a universal broadband saturable absorber that could successfully compete with graphene or other low-dimension nanomaterials.

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In this work we present for the first time, to the best of our knowledge, a stretched-pulse mode-locked fiber laser based on topological insulator. As a saturable absorber (SA) a ~0.5 mm thick lump of antimony telluride (Sb2Te3) deposited on a side-polished fiber was used. Such a SA introduced 6% modulation depth with 43% of non-saturable losses, which is sufficient for supporting stretched-pulse mode-locking. The ring laser resonator based on Er-doped active fiber with managed intracavity dispersion was capable of generating ultrashort optical pulses with full width at half maximum (FWHM) of 30 nm centered at 1565 nm. The pulses with duration of 128 fs were repeated with a frequency of 22.32 MHz.

The paper summarizes the recent achievements in the area of ultrafast fiber lasers mode-locked with so-called lowdimensional nanomaterials: graphene, topological insulators (Bi 2 Te 3 , Bi 2 Se 3 , Sb 2 Te 3), and transition metal sulfide semiconductors, like molybdenum disulfide (MoS 2). The most important experimental achievements are described and compared. Additionally, new original results on ultrashort pulse generation at 1.94 μm wavelength using graphene are presented. The designed Tm-doped fiber laser utilizes multilayer graphene as a saturable absorber and generates 654 fs pulses at 1940 nm wavelength, which are currently the shortest pulses generated from a Tm-doped fiber laser with a graphene-based saturable absorber.

Passive harmonic-mode locking of erbium-doped fiber laser with atomic multilayer graphene is presented. The laser could operate at several harmonics (from 2nd to 21st) of the fundamental repetition frequency of the ring resonator (106 MHz). The highest achieved repetition rate was 2.22 GHz (which corresponds to the 21st harmonic) with sub-picosecond pulse durations and over 40 dB of the supermode noise suppression. The saturable absorber was formed by multilayer graphene, mechanically exfoliated from pure graphite block through Scotch-tape and deposited on the fiber ferrule.

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