Out of 247 traditional Chinese medicines (TCM) investigated, a proportion were contaminated with arsenic (5-15%), lead (approximately 5%), and mercury (approximately 65%). Some preparations exceeded the tolerable daily intake (TDI) for males and females for arsenic (4 and 5 products, respectively), lead (1 and 2 products), and mercury (5 and 7 products). These exceedances were as high as 2760-fold, which posed a potential danger to public health. As many users are known to self-prescribe, there is a substantial risk of poisoning from the consumption of these contaminated TCM.
JA sensitive and specific method for the determination of total available Ag-tetrahydrocannabinol in fiber hemp varieties is described. The method was used for the regulatory purposes in which the detection of higher than the maximum allowed concentration of the psychoactive cannabinoid, Ag-tetrahydrocannabinol, in industrial fiber hemp would result in cancellation of the grower's license. Cannabinoids were extracted from dry leaf powder into hexane containing internal standard chrysene-dl~ using sonication. Ag-Tetrahydrocannabinoi in the extract was separated by gas chromatography and quantitated by mass spectroscopy. A linear calibration range extending to 40 ppm and a limit of detection of 0.2 ng were obtained by using the total ion current mode of detection.
The potential of using a combination of normal and reverse phase thin-layer chromatography for the comparison of disperse, acid, and reactive dyes extracted from textile fibers of forensic science origin was examined. For disperse and acid dyes, the use of a normal silica gel and a reverse phase system was shown to provide a pair of systems of low correlation. In contrast, the use of two silica gel systems provided a pair of highly correlated systems that possibly offered little more additional information than a single system. A suitable reverse phase system for the separation of reactive dyes was not found. The various pairs of silica gel systems tested for reactive dyes were all shown to be highly correlated.
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