On cooling, needle crystals separated which, after recrystallization from alcohol, gave 0.5 g. of light cream-colored needles which melted at 223°. The analytical data were satisfactory for the monofurfuryl ether of the diol.
n
‐Butyl phosphate
reactant: 153 g. (91 cc., 1 mole) of phosphorus oxychloride
product:
n
‐butyl phosphate
product:
n
‐propyl ester
product:
sec.
‐butyl ester
product:
n
‐amyl ester
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