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Die Umsetzung des Phosphinchlorids (II) mit H2S führt abhängig von den Reaktionsbedingungen zu dem Diastereomerengemisch des Diphosphinmonosulfids (Ia)/(Ib) und dem Phosphinsulfid (Ic) oder nur zu (Ic).
255ChemInform Abstract The sodium phosphites (Ia) and phosphinates (Ib) react with the chloroalkenes (II), (IV), (VI), (VII), and (IX) or the chloroacetylenes (X) to produce the oligophosphinates and phosphonates (III), (V), and (VIII). The results of the acidic hydrolysis of these compounds are described in the original paper.
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