A control system for tracing the reference reheating curves of individual steel slabs in continuous furnaces is presented. The system enables the predefined, controllable reheating of slabs in a furnace. The slab temperatures are obtained by the simulation of a mathematical model of the slab‐reheating process. The interior of the continuous furnace is divided into six control zones. The individual zone temperatures are adjusted by the control system in such a way that the temperatures of the slabs in the zone are as close as possible to the desired slab temperatures. To take into account delays in the production line and to synchronize the furnace with the rolling mill's capacities, a time shift of the reference reheating curves and a prolonged drop‐out interval are introduced.
Mathematical descriptions of true stress/true strain curves, experimentally obtained on cylindrical specimens under hot compressive conditions, are of great importance and are widely investigated. An additional black-box modelling approach using transfer functions (TF) is tested. For tested 51CrV4 steel, a TF of third order is employed for description of true stress (output) depending on the strain rate (input). Sets of TF coefficients are determined using numerical optimization techniques for each testing temperature and strain rate. To avoid scattering of TF parameters, time in Laplacian transformation is replaced with strain, while TF input is the strain rate. Obtained models cover deformations starting practically from zero to 0.7. Average absolute relative error for models based on TF of the third order and of the second order are 0.93% and 3.64%.
For Inconel 625, where the γ” and δ phases precipitate, the influence of prior hot rolling on the process is not well covered. The influence of segregation bands and prior hot rolling on the precipitation of secondary phases during aging at 750 °C for different times was investigated. Prior hot-rolling was conducted on a hot rolling mill at 1050 °C and 1150 °C with three different deformation levels. The hot rolled samples were aged at 750 °C for 1, 5, 25 and 125 h. The γ″ precipitated in both the deformed and recrystallized grains in the segregation bands containing a high concentration of niobium and molybdenum and a lower concentration of nickel, chromium and iron. The opposite was observed between the segregation bands where no γ″ precipitate was found. There was a smooth transition in the density and the size of the γ″ particles in the deformed grains at the border of the segregation bands, while a more complex transition occurred in the recrystallized grains. This occurred in the area where the average niobium concentration decreased from 4.5 to 2.7 wt. %, which influenced the mechanical properties.
The 2101 lean duplex stainless steel (LDX) was designed mainly for lightweight constructions and as a more economical substitute for the dominating stainless-steel grades. Compared with other duplex stainless steels, the corrosion resistance and costs of processing the 2101 duplex stainless steel are usually worse, as the Ni and Mo contents are lower; it is compensated by higher N and Mn contents to stabilize the austenite. At lower test temperatures the precipitation of different phases was observed, so different annealing experiments were conducted to further investigate the occurrence of precipitation. As the composition of lean duplex stainless steel differs from that of conventional duplex stainless steels, a different aging behaviour is expected. The embrittlement of 2101 lean duplex stainless steel occurs at approximately 700°C to 750°C, because of the precipitation of the deleterious Cr2N and M23C6 at the d/g and d/ d interfaces, which begins after a few minutes of aging. These temperatures of the nitride precipitations are crucial to the cracking during the end of hot-working operations, which should stop at higher temperatures. The purpose of the research was to qualitatively analyse the phases in lean duplex stainless steel after thermal aging. Optical microscopy (OM), scanning electron microscopy (SEM) and electron-backscatter diffraction (EBSD) were used to investigate the structural stability and the chemical compositions of the phases.
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