Titanium possesses a unique ability to bind with bone and living tissue, making it an ideal material for orthopedic implants such as knee and hip replacements. Because of the strength to weight ratio, hermeticity, biocompatibility and light weight makes titanium and its alloy the best choice for implant. The main goal focused on studying the influence of surface coating of some titanium base alloys by Nano (ZrO2&Y2O3) to the surface roughness of implant alloys. Preparation of samples was accomplished by using powder technology technique, in which the raw materials was pure titanium, 10%cobalt,50% nickel, and 30% tantalum powders. The samples were cleaned by ultrasonic device the surface pre- treated by chemical etching, then deposition of nano (ZrO2 with Y2O3) accomplished by pack cementation process. After samples characterization by (X-ray diffraction, hardness test, porosity percentage and Surface roughness). The result showed that diffraction patterns gained for the samples were the phases developed as a result of sintering and after deposition, There are likely no presents of pure metals that prove the time and temperature of sintering utilized in this work results in full sintering reactions, the XRD patterns of samples after (ZrO2,Y2O3) deposition by pack cementation process. It is obvious that Amorphous behavior was observed in the XRD after deposition nearly at 2θ (15.799) for all samples. It is evident that the porosity percent of the samples after (ZrO2, Y2O3) deposition was largely decreases due to the pack cementation process. There was considerable increasing in hardness value, finally the roughness values obtained from the AFM it was found that there are large changes in the roughness value of samples after coating due to full the surface by Nano ceramic material deposition.
The ultimate goal of using biomaterials is to improve human health by restoring the function of natural living tissues and organs in the body. The present work aims to modify the composite coating layer properties by using two different types of bioactive reinforcing materials (biotin and hydroxyapatite) particles in different percentages (5% and 10%). Coatings were applied onto commercially pure Ti, SS 316 L, and SS 304 substrates by the dip-coating method. Characterization of samples includes microstructure observation by field emission scanning electron microscopy (FE-SEM), contact angle measurement (wettability), and MTT. The results show the addition of metallic particles (bioparticles) (hydroxyapatite particles, biotin) at 5 Vol. % improved the whole properties of composite materials. Using different particles’ scale size aids to enhance the combinations in the alginate matrix producing a dual effect on composite film properties. In addition, the inclusion of metallic particles has to increase the wettability by reducing the contact angle. At the same time, MTT graphs revealed that after 3 days of exposure in MG-63 cells, 316 L SS alloys’ surface following pack adhesion became more active.
Titanium has a good ability to attach to bone and living tissue, making it a perfect material for orthopedic implants. Because of the combination of high resistance to corrosion, biocompatibility and excellent mechanical properties. This work aims to study the Modifications of various base titanium implant samples producing by using powder technology (Ti-pure, Ti-45 % Ni, Ti10 % Co, and Ti-30 % Ta) by deposition of Nano Zirconia and yttria powders (70 % and 30% ). Chemical pretreatment carried out to prepare the implant surface before deposition, while the deposition process accomplished by pack cementation. The Characterizations of samples accomplished before and after the surface treatment, which includes: microstructure observation, x-ray diffraction (XRD), MTT Assay (cell viability) and MTT assay (cell adhesion). From the SEM All samples Show that Nano Zirconia and yttria were homogeneously put on the surface and fully covered it which resulted in a substantial modification in surface morphologies. From XRD patterns the peaks slightly shifted to the low angle side also amorphous behavior was observed. From MTT graphs it was found that the titanium alloys surface after pack cementation became more active after 3 days of exposure in MG-63 cells and there was a remarkable increase in cell viability and cell attachment compared with untreated samples.
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