The effect of cooling rates during a double stage solution treatment (DSST) on the volume fraction of the massive phase (αm) in Ti-6Al-4V alloy was successfully confirmed in the present study. The morphology of Ti-6Al-4V alloy depends on the cooling rates during the cooling from the β region. The αm, which has a transformation characteristic between martensite (α′) and α diffusion, is reported to be a potential method for obtaining a fine lamellar α/β by thermal decomposition. The different fraction of αm was found after DSST with the first stage was conducted above the β-transus temperature at 1050 °C, followed by second annealing at different temperatures in the α+β region. It was found that the formation of αm exists in a specific temperature region. A longer period in this region, which was calculated based on different cooling rates during DSST, will increase the fraction of αm in the specimen. All specimens after DSST contain αm with the α width of approximately 1μm and white-dot particles, which is predicted to be V-enriched precipitates. The DSST can be a potential method for producing a high fraction of αm, which can be thermally decomposed into a fine lamellar α/β, introducing a Ti-6Al-4V alloy with superior mechanical properties.
The alteration in phase morphology of Ti-6Al-4V alloy fabricated using directed energy deposition (DED) was investigated in this study. Owing to the fast cooling rate during DED, the specimen exhibited the diffusionless transformation products of martensite (α′) and massive (αm) phases. In the top layer, the α′ exhibited a needle-like morphology with the width of approximately 0.94 μm. Meanwhile, the αm presented a lamellar structure with α thickness of nearly 0.98 μm. In contrast, the morphology of α′ and αm started to decompose into α+β phase in the bottom layer. Furthermore, the hardness values increased with higher deposition layers. These phenomena could be explained by the effect of repetitive heating, as the nature of DED method during the depositing of new layers. Moreover, it was observed the α thickness of αm in the bottom layer was finer than that in the top layer due to the higher cooling rate.
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