This work establishes a simple method for synthesising layered double hydroxides (LDHs) powders with coprecipitation. The characteristics of the samples were investigated y X-ray diffraction (XRD), scanning electron microscopy (SEM) and spectrophotometer UV–Vis (DRS). Non-uniform distribution was shown for LDHs samples by SEM. Photocatalytic efficiencies were tested using methylene blue (MB) dye as a model contaminant under UV irradiation. In particular, Zn–Al-Ti LDH exhibited an excellent performance towards MB degradation compared with commercial TiO2 nanoparticles. Methylene blue removal percentage was reached at almost 100%, whereas commercial TiO2 reached a removal rate of only 66% under the same conditions within 20 min. The aim of the current work is to prepare Zn-Al-Ti layered double hydroxides nanocomposite and to evaluate their photocatalytic activity in the removal of methylene blue under UV irradiation.
Abstract. Solid waste generated during mining is one of the major environmental problems associated with this industrial activity. The best solution to overcome the environmental impact of this waste is to find recycling facilities in mass-produced products that can absorb the large quantities of these available byproducts. The present study shows the feasibility of using the coal waste of Moroccan Jerrada mining in the production of ecological brick. The first step consists of consecutive stages of crushing, grinding and heating at 650°C of the coal waste with a small amount of lime in order to promote the reactive products of elaborated binders. The second step of the process consists of mixing treated coal waste with a small amount of marble dust, sand, gravel, and water, then pressed and dried at room temperature to manufacture a laboratory ecofriendly bricks. The mechanical strength and thermal conductivity are investigated.
Solid waste generated during mining is one of the major environmental problems associated with this industrial activity. The best solution to overcome the environmental impact of this waste is to find recycling facilities in mass-produced products that can absorb the large quantities of these available byproducts. The present study shows the feasibility of using the coal waste of Moroccan Jerrada mining in the production of ecological brick. The first step consists of consecutive stages of crushing, grinding and heating at 650°C of the coal waste with a small amount of lime in order to promote the reactive products of elaborated binders. The second step of the process consists of mixing treated coal waste with a small amount of marble dust, sand, gravel, and water, then pressed and dried at room temperature to manufacture a laboratory ecofriendly bricks. The mechanical strength and thermal conductivity are investigated.
Recently, the belitic cements with low alite content were the subject of several research works which aimed to replace the Ordinary Portland Clinker (OPC) for ecological reasons (reduction of CO2 emissions), so to understand the reactivity of this cement, the hydration study of the C2S “dicalcium silicate” phase is primordial research step. As well for a clean environment, the TiO2 photocatalyst has been extensively applied in the science of building materials because of its ability to degrade the cement surface pollutants. New photocatalyst based layered double hydroxides (LDH) associated with zinc, aluminium and TiO2 was introduced to increase the compatibility with mortars. The present work is subjected to investigate the effect of the layered double hydroxides on the hydration of C2S in following the evolution of hydration by X-ray diffraction at 2, 7, 28 and 90 days and analyzing the calcium/silicon ratio of different formed hydrates.
In recent years, waste recycling has become a key issue in construction materials science for achieve the goal of sources of raw materials. The aim of this study is to use waste glass as source of SiO2 oxide and mussel shells consisting essentially of calcium carbonate as starting materials to synthesize belite rich cement. The elaborated clinker is chemically and structurally related to β-Ca2SiO4, by heat solid state activation. After grinding, the raw materials are mixed and heated up to 1050°C. The samples are characterized by X-ray diffraction (XRD) and Fourier Transformed Infrared spectroscopy (FT-IR). The mechanical strength of some sample was measured for 28 and 72 days. The results show the different mineralogical stapes of formation of clinker, the state reaction method allows the elaboration of a cementitious material by a simple heat treatment at relatively low temperature and low release of CO2. The hydration products are also identified by XR diffraction at 2, 7, 28 and 72 days.
Abstract. This work establishes a simple method for synthesising layered double hydroxides (LDHs) powders with coprecipitation. The characteristics of the samples were investigated y X-ray diffraction (XRD), scanning electron microscopy (SEM) and spectrophotometer UV-Vis (DRS). Non-uniform distribution was shown for LDHs samples by SEM. Photocatalytic efficiencies were tested using methylene blue (MB) dye as a model contaminant under UV irradiation. In particular, Zn-Al-Ti LDH exhibited an excellent performance towards MB degradation compared with commercial TiO 2 nanoparticles. Methylene blue removal percentage was reached at almost 100%, whereas commercial TiO 2 reached a removal rate of only 66% under the same conditions within 20 min. The aim of the current work is to prepare Zn-Al-Ti layered double hydroxides nanocomposite and to evaluate their photocatalytic activity in the removal of methylene blue under UV irradiation.
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