Se0.9In0.1 samples were prepared from their highly pure constituents, by ice‐water quenching from the melts. Structural characterization using XRD and DTA has revealed a stable phase consisting of some crystalline clusters embedded in a glassy matrix with a single glass transition (Tg) at a temperature 320 K, an onset exothermic crystallization peak at 361 K, and a melting endotherm with a melting point at 473 K. The dc (ohmic contact region) and ac (50 Hz–80 kHz) conductivities were measured under vacuum as a function of temperature (from T < Tg down to LN2) for massive samples, 0.3–0.6 mm thick. Results of the space‐charge‐limited current and the electrical characteristics of both dc and ac conduction are given and discussed in the light of the temperature dependence of the conduction mechanism.
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