ABSTRAK Salah satu upaya untuk menjaga persediaan air yaitu dengan cara menurunkan parameter air laut agar memenuhi parameter air tawar menggunakan metode elektrokoagulasi. Penelitian ini bertujuan untuk mempelajari pengaruh waktu proses elektrokoagulasi terhadap penurunan TDS, kekeruhan, kadar Cl, dan kadar Fe. Selain itu, untuk mengetahui perbandingan antara elektroda Al dan Fe. Air laut diambil dari Pantai Pelabuhan Ratu. Elektroda yang digunakan adalah Al dan Fe dengan ukuran 15x10 cm2. Tegangan yang digunakan yaitu 5 volt atau rapat arus sebesar 0,137 A/dm2 dengan waktu proses 15, 30, 45, dan 60 menit serta volume bahan bakunya 4 Liter. Penelitian dengan waktu proses 30 menit dan proses pengendapan selama satu hari mampu menurunkan kekeruhan hingga 2,28 NTU (55,07%); TDS hingga 1.010 mg/L (3,71%); kadar Cl hingga 271,98 mg/L (3,52%); dan kadar Fe 0,05 mg/L (40,65%). Proses elektrokoagulasi menggunakan elektroda aluminium lebih baik dibandingkan elektroda besi pada waktu proses 30 menit. ABSTRACT One of the efforts to maintain water supply is by lowering seawater parameters to meet freshwater parameters using the electrocoagulation method. This study aims to study the effect of electrocoagulation process time on the decrease in TDS, turbidity, Cl content, and Fe content. In addition, to determine the comparison between Al and Fe electrodes. Seawater is taken from Pelabuhan Ratu Beach. The electrodes used are Al and Fe with a size of 15x10 cm2. The voltage used is 5 volts or a current density of 0,137 A/dm2 with processing times of 15, 30, 45, and 60 minutes and the volume of the raw material is 4 liters. Research with a processing time of 30 minutes and sedimentation for one day was able to reduce turbidity up to 2,28 NTU (55,07%); TDS up to 1.010 mg/L (3,71%); Cl content up to 271,98 mg/L (3,52%); and Fe content of 0,05 mg/L (40,65%). The electrocoagulation process using aluminum electrodes was better than iron electrodes at a processing time of 30 minutes.
Eksplorasi minyak bumi dari sumur-sumur yang sudah tua menghasilkan minyak dengan kandungan air tinggi. Hydrocyclone suatu alat yang berfungsi untuk pemisahan cair-cair berdasarkan perbedaan berat jenis setiap komponen. Pemisahan ini terjadi dikarenanakan adanya gaya sentrifugal dan gaya gravitasi yang dihasilkan dari bentuk hydrocyclone yang seperti kerucut. Perancangan dan pembuatan hydrocyclone menghasilkan alat dengan spesifikasi sebagai berikut : diameter pipa masukan : 25,4 mm, diameter cylindrical section : 120 mm, tinggi cylindrical section : 120 mm, tinggi cone section : 600 mm, diameter pipa overflow : 25,4 mm, diameter pipa underflow : 25,4 mm. Laju alir optimum untuk pemisahan air-minyak tanah pada hydrocyclone adalah 91,8 liter/menit dengan kadar minyak tanah di overflow sebesar 11,4% dan kadar minyak tanah di underflow sebesar 3%.Petroleum exploration from old wells produces oil with a very high water content. Hydrocyclone is a device that functions for liquid-liquid separation based on differences in specific gravity of each component. This separation occurs due to the presence of centrifugal forces and gravitational forces resulting from cone-like forms of hydrocyclone. The design and manufacture of hydrocyclone produces tools with the following specifications: input pipe diameter: 25.4 mm, cylindrical section diameter: 120 mm, high cylindrical section: 120 mm, cone section height: 600 mm, overflow pipe diameter: 25.4 mm, underflow pipe diameter: 25.4 mm. The optimum flow rate for the separation of water-kerosene on hydrocyclone is 91.8 liters / minute with the level of kerosene in overflow of 11.4% and the level of kerosene in underflow of 3%.
Abstract. Contact Glow Discharge Electrolysis (CGDE) method is one of Plasma Electrolysis technology which has been approved to degrade organic waste water because it is very productive in producing hydroxyl radical. This study aims to degrade Remazol Red by CGDE method and evaluate important parameters that have influent in degradation process of Remazol Red in Batik dye waste water in batch system. The kind of electrolyte (acid and base) and the addition of metal ion such as Fe 2+ have affected Remazol Red degradation percentage. Ultraviolet-Visible (UV-Vis) absorption spectra were used to monitor the degradation process. The result of study showed that percentage degradation was 99.97% which obtained by using NaCl 0.02 M with addition Fe 2+ 20 ppm, applied voltage 700 volt, anode depth 0.5 cm, initial concentration of Remazol Red 250 ppm and the temperature of solutions was maintained 50-60 ˚C.
ABSTRAK Perkembangan baterai tak luput dari kebutuhan energi yang kian meningkat. Meskipun sumber energi tidak terpaku pada baterai, namun baterai banyak diminati karena dapat menampung cukup banyak energi, relatif aman, dan bersifat portable. Penelitian ini bertujuan untuk mensintesa dan mengetahui karakteristik salah satu jenis katoda baterai lithium-ion yaitu Lithium Iron Phosphate (LiFePO4) dengan variasi mol reagent berdasarkan perbandingan stoikiometri dan suhu proses kalsinasi 600°C, 700°C, dan 800°C selama 3x3 jam menggunakan metode solid state reaction dengan Li2SO4.H2O, FeSO4.7H2O, dan KH2PO4 sebagai reagent. Produk hasil kalsinasi 800°C dengan variasi 0.1 mol dijadikan sampel untuk dianalisa dan dikarakterisasi karena memiliki penurunan berat endapan BaSO4 tertinggi. Hasil karakterisasi menggunakan FTIR menunjukan gugus fungsi P-O yang cukup kuat, sementara hasil karakterisasi menggunakan SEM/EDX menunjukan partikel yang terbentuk memiliki ukuran sekitar 160nm hingga 14µm dan terdapat atom S yang merupakan impurities dalam produk. Pola difraksi hasil uji XRD menunjukan terbentuknya sejumlah fasa seperti LiFePO4, LiFeP2O7, dan Li3PO4. ABSTRACT The development of batteries is inseparable from the increasing energy needs. Although energy sources are not available for batteries, batteries are in great demand because they can store a lot of energy, are relatively safe, and are portable. This study aims to synthesize and determine the characteristics of one type of lithium-ion battery cathode, namely Lithium Iron Phosphate (LiFePO4) with various mole reagents based on stoichiometric ratios and calcination process temperatures of 600oC, 700oC, and 800oC for 3x3 hours using the solidstate reaction method with Li2SO4.H2O, FeSO4.7H2O, and KH2PO4 as reagents. The 800oC calcined product with 0.1 mol variation was sampled for analysis and characterization because it had the highest weight loss of BaSO4 deposits. The results of characterization using FTIR showed that the functional group P-O are quite strong, while the results of characterization using SEM/EDX showed that the particles formed had a size of about 160nm to 14µm and contained S atoms which were impurities in the product. The diffraction pattern of XRD test results shows the formation of phase numbers such as LiFePO4, LiFeP2O7, dan Li3PO4.
Accumulation Oil Palm Empty Bunches (TKKS) cause environmental problems if not solved. TKKS has a high cellulose composition, so it can be used as nanocellulose which has a higher value. The process of making nanocellulose from TKKS through the isolation stage of α-cellulose with a delignification process using Sodium Hydroxide (NaOH) 17.5% (b/v) at 80°C, bleaching using Hydrogen Peroxide (H2O2) 10% (v/v), hydrolysis using sulfuric acid and drying using freeze drying at a heating temperature of 53°C for 7 hours. Cellulose yield produced from the isolation process of α-cellulose from TKKS was 20.8%. The results of drying process will reduce the aggregation of particles in the nanocellulose produced, so that nanocellulose is produced at 160-298 nm.
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