Brillouin optical time-domain analysis (BOTDA) requires frequency mapping of the Brillouin spectrum to obtain environmental information (e.g., temperature or strain) over the length of the sensing fiber, with the finite frequency-sweeping time-limiting applications to only static or slowly varying strain or temperature environments. To solve this problem, we propose the use of an optical chirp chain probe wave to remove the requirement of frequency sweeping for the Brillouin spectrum, which enables distributed ultrafast strain measurement with a single pump pulse. The optical chirp chain is generated using a frequency-agile technique via a fast-frequency-changing microwave, which covers a larger frequency range around the Stokes frequency relative to the pump wave, so that a distributed Brillouin gain spectrum along the fiber is realized. Dynamic strain measurements for periodic mechanical vibration, mechanical shock, and a switch event are demonstrated at sampling rates of 25 kHz, 2.5 MHz and 6.25 MHz, respectively. To the best of our knowledge, this is the first demonstration of distributed Brillouin strain sensing with a wide-dynamic range at a sampling rate of up to the MHz level.
We present a slope-assisted BOTDA system based on the vector stimulated Brillouin scattering (SBS) and frequency-agile technique (FAT) for the wide-strain-range dynamic measurement. A dimensionless coefficient K defined as the ratio of Brillouin phase-shift to gain is employed to demodulate the strain of the fiber, and it is immune to the power fluctuation of pump pulse and has a linear relation of the frequency detuning for the continuous pump and Stokes waves. For a 30ns-square pump pulse, the available frequency span of the K spectrum can reach up to 200MHz, which is larger than fourfold of 48MHz-linewidth of Brillouin gain spectrum. For a single-slope assisted BOTDA, dynamic strain measurement with the maximum strain of 2467.4με and the vibration frequency components of 10.44Hz and 20.94Hz is obtained. For a multi-slope-assisted BOTDA, dynamic measurement with the strain variation up to 5372.9με and the vibration frequency components of 5.58Hz and 11.14Hz is achieved by using FAT to extend the strain range.
We propose and demonstrate a dynamic Brillouin optical fiber sensing based on the multi-slope assisted fast Brillouin optical time-domain analysis (F-BOTDA), which enables the measurement of a large strain with real-time data processing. The multi-slope assisted F-BOTDA is realized based on the double-slope demodulation and frequency-agile modulation, which significantly increases the measurement range compared with the single- or double- slope assisted F-BOTDA, while maintaining the advantage of fast data processing and being suitable for real-time on-line monitoring. A maximum strain variation up to 5000με is measured in a 32-m fiber with a spatial resolution of ~1m and a sampling rate of 1kHz. The frequency of the strain is 12.8Hz, which is limited by the rotation rate of the motor used to load the force on the fiber. Furthermore, the influence of the frequency difference between two adjacent probe tones on the measurement error is studied theoretically and experimentally for optimization. For a Brillouin gain spectrum with a 78-MHz width, the optimum frequency difference is ~40MHz. The measurement error of Brillouin frequency shift is less than 3MHz over the whole measurement range (241MHz).
We demonstrate a high-spatial-resolution fast Brillouin optical time-domain analysis (BOTDA) for distributed dynamic strain measurement based on differential doublepulse and second-order sideband of modulation. The frequency-agility probe wave is obtained from the second-order sideband of the modulated light by using the microwave signal from a wideband arbitrary waveform generator (AWG), which reduces the bandwidth requirement of the AWG by half to $5.5 GHz. The differential double-pulse scheme is proposed to improve the spatial resolution while keeping the capability of dynamic measurement. In experiment, a spatial resolution of 20 cm is achieved by using a 52/50 ns differential double-pulse, and the distributed vibration measurement is demonstrated over a 50-m Panda polarization-maintaining fiber observing the vibration frequency of up to 50 Hz. With only five averages, the standard deviation of the strain accuracy is measured to be 14 ".
Surface‐enhanced Raman spectroscopy (SERS) was used for rapid detection of sodium thiocyanate in milk employing silver aggregates as active substrate. Silver nanoparticles were induced to silver aggregates by trichloroacetic acid (TCA). The limit of detection (LOD) for sodium thiocyanate was 10−2 µg ml−1 in water with an analytical enhancement factor of 5.4 × 106. The silver aggregates represent good reproducibility and stability. Good linear relationship was obtained for sodium thiocyanate in milk at concentration ranges from 0.1 to 10 µg ml−1 (R2 = 0.995). Using TCA as protein precipitator, silver colloid would aggregate spontaneously when mixing with samples during SERS measurement without the need of additional aggregating agent. The simple pretreatment procedures and analytical methods are less time consuming (<10 min) and environmentally friendly, making the proposed method much practical for in situ detection of sodium thiocyanate in market milk. Copyright © 2014 John Wiley & Sons, Ltd.
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