The analysis of phenols in samples of plant and food origin attracts considerable attention. However, sample handling is often an ignored feature of the analysis. This review highlights the importance of sample extraction in an analysis and the problems that can arise during this step. Many questions remain unanswered and there is a need to more carefully validate extraction efficiencies. Although many new procedures have been developed the use of traditional techniques still dominates.
The volatile profile of virgin olive oils was established using SPME and gas chromatography(-mass spectrometry). The major volatile in approximately 50% of the oils was E-hex-2-enal in contrast with European oils. The minor contribution of C5 compounds to the volatile profiles also contrasted with data on European oils. Hierarchical Cluster Analysis (HCA) implicates variety as the single-most important factor in determining volatile profile whilst malaxation time and temperature exerted a minor secondary effect on the volatile profile. #
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