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This work aimed to enhance the creep resistance of Ti-6Al-4V alloy treated by plasma nitriding. The nitriding was performed on specimens with a Widmanstätten microstructure for four hours at 690 °C under a gas atmosphere containing Ar:N2:H2 (0.455:0.455:0.090). X-ray diffraction analysis showed that the ε-Ti2N and δ-TiN formed on the nitrided sample, in addition to the α-Ti and β-Ti matrix phases. The layer thickness of this sample was about 1 µm. Hot tensile tests were performed in the temperature range of 500 to 700 °C on nitrided and non-nitrided samples, which indicated an increased strength of the nitrided samples. The same temperature range was used for the creep tests in a stress range of 125 to 319 MPa. The plasma-nitrided samples exhibited better creep resistance when compared to the untreated samples. This result was demonstrated by the decreased secondary creep rate and the increased final creep time. This improvement in the creep resistance appeared to be associated with the formation of the nitrided layer, which worked as a barrier to oxygen diffusion into the material and due to the formation of a surface residual compressive stress.

Inconel 625 is a nickel-based alloy that is mainly used in high-temperature applications. Inconel 625 exhibits an unstable plastic flow at elevated temperatures characterized by serrated yielding, well-known as the Portevin-Le Chatelier effect. The evaluation of the mechanical properties of Inconel 625 at high temperatures is the aim of this work. The tensile tests were executed in temperatures ranging from room temperature to 1000 °C with strain rates of 2 × 10−4 to 2 × 10−3 s−1. The creep tests were executed in the temperature range of 600–700 °C and in the stress range of 500–600 MPa in a constant load mode. The optical and scanning electron microscopes were used for surface fracture observation. In the curves obtained at 200–700 °C the serrated stress-strain behavior was observed, which was related to the dynamic strain aging effect. The yield strength and the elongation values show anomalous behavior as a function of the test temperature. An intergranular cracking was observed for a specimen tensile tested at 500 °C that can be attributed to the decohesion of the carbides along the grain boundaries. The fracture surface of the specimen tensile tested at 700 °C showed the predominance of transgranular cracking with tear dimples with a parabolic shape.

Aluminum alloys have low specific weight, relatively high strength and high corrosion resistance and are used in many applications. Aluminum Alloy 2024 is widely used for aircraft fuselage structures, owing to its mechanical properties. In this investigation, Aluminum Alloy 2024 was given solid solution treatments at 495, 505, and 515°C followed by quenching in water. It was then artificially aged at 190 and 208°C. Subsequently, hardness measurements, tensile tests as well as impact and fatigue tests were carried out on the heat treated alloys to determine the mechanical properties. The tensile and hardness tests revealed similar mechanical properties for specimens of this alloy that were given the three solid solution treatments. Aluminum Alloy 2024 specimens that were solid solution treated at 515°C and artificially aged at 208°C for 2h exhibited the highest yield and tensile strength. In general, the increase in strength was accompanied by a decrease in ductility. Cyclic fatigue studies were conducted with symmetric tension-compression stresses at room temperature, using a bending-rotation test machine. The alloy solution heat treated at 515°C and aged at 208°C/2h was fatigue tested at constant frequency. The relation between stress amplitude and cycles to failure was established, enabling the fatigue strength to be predicted at more than 7.8x106cycles, with maximum stress of 110.23 MPa. The fracture surfaces of specimens that failed after fewer cycles showed mainly precipitates and micro voids, whereas specimens that fractured after a higher number of cycles indicated that cracks initiated at the surface. The high cycle fatigue fracture surfaces revealed pores that could be due to precipitates from the matrix.

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A superalloy is an alloy developed for elevated temperature service, where relatively severe mechanical stressing is encountered, and where high surface stability is frequently required. High temperature deformation of Ni-base superalloys is very important since the blades and discs of aero engine turbine, because need to work at elevated temperature for an expected long period. The nickel-base alloy Inconel 718 has being investigated because it is one of the most widely used superalloys. The objective of this work was to evaluate the creep behavior of the Inconel 718 focusing on the determination of the experimental parameters related to the primary and secondary creep states. Constant load creep tests were conducted with at 650, 675 and 700°C and the range of stress was from 625 to 814 MPa to according to ASTM E139 standard. The relation between primary creep time and steady-state creep rate, obeyed the equation for both atmospherics conditions at 650, 675 and 700°C. The microstructural characterization employing the technique of scanning electron microscopy has been a valuable tool for understanding the mechanisms of creep.

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