In this paper, Fe-OCAP/PU blends were prepared. The mechanical properties and thermal stability of the samples were studied by tensile tests and thermogravimetric analysis, respectively. Results showed that the mechanical properties and thermal stability of the samples were improved with the increase of Fe-OCAP content. The antibacterial property of Fe-OCAP and Fe-OCAP/PU films was investigated by agar diifusion method and shake flask method, respectively. Fe-OCAP and Fe-OCAP/PU films showed efficient antibacterial activity againstS.aureus.
A nanocomposite catalyst was prepared from immobilization of aluminum oxide hydroxide onto the attapulgite for synthesis of Poly (ethylene terephthalate) (PET). Differential scanning calorimetry (DSC) analysis was used to investigate the crystallization properties of PET obtained by using the different catalysts, and the results showed that PET obtained by using the as-prepared catalyst exhibited higher crystallization crystallizability under applied conditions.
The aim of the current study was to improve the knowledge of the gelation process of injectable thermosensitive hydrogels comprising chitosan (CS) and β-glycerophosphate disodium salt (β-GP). The sol-gel transition process was precisely tracked by means of rheological measurement, in which the viscosity changed considerably with gelation time and temperature. The zero-order kinetics model was assumed to adequately describe the extent of gelation reaction. The reaction rate constant increased continuously with the increasing temperature and β-GP concentration. According to Arrhenius equation, the activation energies of gelation reaction for the chitosan injectable hydrogels were calculated as 64.38 KJ/mol, 101.68 KJ/mol and 140.92 KJ/mol for the samples containing 4% w/v, 6% w/v and 8% w/v of β-GP, respectively. It could be an effective way to study the gelation dynamics of injectable hydrogels, and provide references for clinical practice.
Attapulgite (AT)-based nanofibrous membranes (NFMs) were fabricated via a facile papermaking procedure, and the AT-based NFMs were sintered at three different temperatures (240 °C, 400 °C, and 600 °C). The effect of sintering temperature on the structure and properties, such as specific surface area, pore size distribution, porosity, mechanical property, pure water fluxes of AT-based NFMs, were investigated. The results showed that average pore size, total pore volume, and porosity of AT-based NFMs increased with increasing of the sintering temperature, while specific surface area and flexural strength of AT-based NFMs decreased. The optimal sintering temperature for AT-based NFMs was 400 °C. In addition, it was also found that the swelling degree of AT-based NFMs in aqueous solutions was suppressed and the pure water fluxes of AT-based NFMs were improved by sintering process.
As a multi-resolution signal decomposition and analysis technique, the wavelet transforms have been already introduced to vibration signal processing. In this paper, a comparison on the time-scale map analysis is made between the discrete and the continuous wavelet transform. The orthogonal wavelet transform decomposes the vibration signal onto a series of orthogonal wavelet functions and the number of wavelets on one wavelet level is different from those on the other levels. Since the grids are unevenly distributed on the time-scale map, it is shown that a representation pattern of a vibration component on the map may be significantly altered or even be broken down into pieces when the signal has a shift along the time axis. On contrary, there is no such uneven distribution of grids on the continuous wavelet time-scale map, so that the representation pattern of a vibration signal component will not change its shape when the signal component shifts along the time axis. Therefore, the patterns in the continuous wavelet time-scale map are more easily recognised by human visual inspection or computerised automatic diagnosis systems. Using a Gaussian enveloped oscillation wavelet, the wavelet transform is capable of retaining the frequency meaning used in the spectral analysis, while making the interpretation of patterns on the time-scale maps easier.
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