Fracture toughness of six dental porcelains with leucite content ranging from 0 to 22 vol% was evaluated by indentation fracture (IF), surface crack in flexure (SCF), and single edge pre‐cracked beam (SEPB) methods. The results of the IF method were similar to those of the SCF method for all the porcelains investigated. The results of the SEPB were similar to those of the other two methods only for the glassy porcelains, but for leucite‐based porcelains this method resulted in higher values of KIc. Based on microstructure, fractographic analysis, and an additional single edge V‐notched beam test, it was concluded that the pre‐crack size influences the value of KIc for porcelains reinforced by leucite. For design and failure analysis purposes, the KIc determined by SCF method should be preferred, since fracture of dental restorations usually starts from small surface cracks.
The objective of this work was to evaluate biaxial-flexural-strength (σ f ), Vickers hardness (HV), fracture toughness (K Ic ), Young's modulus (E), Poisson's ratio (ν) and porosity (P) of two commercial glass-ceramics, Empress (E1) and Empress 2 (E2), as a function of the hot-pressing temperature. Ten disks were hot-pressed at 1065, 1070, 1075 and 1080 °C for E1; and at 910, 915, 920 and 925 °C for E2. The porosity was measured by an image analyzer software and σ f was determined using the piston-on-three-balls method. K Ic and HV were determined by an indentation method. Elastic constants were determined by the pulse-echo method. For E1 samples treated at different temperatures, there were no statistical differences among the values of all evaluated properties. For E2 samples treated at different temperatures, there were no statistical differences among the values of σ f , E, and ν, however HV and K Ic were significantly higher for 910 and 915 °C, respectively. Regarding P, the mean value obtained for E2 for 925 °C was significantly higher compared to other temperatures.
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