This study evaluated the influence of plastic deformation during hot strip rolling in the size of TiN precipitates in an industrial Ti microalloyed dual phase steel. TiN is usually used for pinning austenitic grain boundaries during recrystallization and its efficiency depends on factors such as size of the precipitates and Ti precipitated fraction. During the slab reheating process, there occurs a partial dissolution of TiN precipitates that subsequently reprecipitates during the hot rolling process. However, this reprecipitation preferentially takes place at crystalline defects which act as nucleation sites. These sites increase with the amount of applied plastic deformation, resulting in smaller precipitates, due to the partial dissolution of larger particles or due to reprecipitation in the nucleation sites. Results indicate a reduction of about 28 % in the average size of the precipitates for samples extracted from hot bands (with deformation) and, therefore, a significant reduction in austenitic grain size, when compared with samples extracted from slabs (with no deformation).
The refinement of microstructure and its homogeneity during controlled hot strip rolling is primarily achieved by controlling the austenite recrystallization before its transformation during accelerated cooling. The paper describes the methodology to determine the deformation conditions favorable for dynamic recrystallization (DRX). Using this methodology it becomes possible to delineate the conditions for postdeformation static and metadynamic recrystallization as well. The work is based on viscoplastic power law formalism applied to steady state flow within wide range of deformation temperatures and strain rates. Two equations of the same form but with different coefficients can be used depending on whether the steady state flow is controlled by dynamic recovery (DRV) or DRX. The transition from DRV-to DRX at the corresponding value of Zener-Hollomon parameter Zt can be viewed as the demarcation between static and metadynamic recrystallization occurring after deformation. The approach is illustrated using low carbon Mn-V steel. Alloying with Cr and especially with Mo suppresses DRX and MDRX as manifested by increasing Zt.
ResumoOs efeitos da temperatura de austenitização, taxa de resfriamento e adições de Cr ou Mo nas transformações de fases de um aço 0,12C-1,70Mn-0,2V, utilizando dilatometria, foi investigado. Os diagramas em resfriamento contínuo de sete aços foram elaborados e as microestruturas foram identificadas utilizando microscopias ótica e eletrônica de varredura. Em temperaturas de austenitização mais elevadas, taxas de resfriamento mais altas e maiores adições de elementos de liga (Cr ou Mo), houve uma elevação significativa da temperabilidade e queda na temperatura Ar3. Uma comparação entre os efeitos do Cr e o Mo também foi realizada, mostrando um efeito mais efetivo do Mo. Foi observada redução na temperatura Ms com o decréscimo da taxa de resfriamento. Não foi observada variação significativa de Ms com o aumento da temperatura de austenitização ou adição de elementos de liga. Palavras-chave: Dilatometria; Transformação de fases; Temperabilidade; Efeitos de Cr e Mo.
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