PURPOSE: This study evaluated the degree of conversion (DC) of four indirect resin composites (IRCs) with various compositions processed in different polymerization units and investigated the effect of thermal aging on the flexural strength and Vicker's microhardness. MATERIALS AND METHODS: Specimens were prepared from four IRC materials, namely Gr 1: Resilab (Wilcos); Gr2: Sinfony (3M ESPE); Gr3: VITA VMLC (VITA Zahnfabrik); Gr4: VITA Zeta (VITA Zahnfabrik) using special molds for flexural strength test (N = 80, n = 10 per group) (25 x 2 x 2 mm(3), ISO 4049), for Vicker's microhardness test (N = 80, n = 10 per group) (5 x 4 mm(2)) and for DC (N = 10) using FT-Raman Spectroscopy. For both flexural strength and microhardness tests, half of the specimens were randomly stored in distilled water at 37 degrees C for 24 hours (Groups 1 to 4), and the other half (Groups 5 to 8) were subjected to thermocycling (5000 cycles, 5 to 55 +/-1 degree C, dwell time: 30 seconds). Flexural strength was measured in a universal testing machine (crosshead speed: 0.8 mm/min). Microhardness test was performed at 50 g. The data were analyzed using one-way and two-way ANOVA and Tukey's test (alpha= 0.05). The correlation between flexural strength and microhardness was evaluated with Pearson's correlation test (alpha= 0.05). RESULTS: A significant effect for the type of IRC and thermocycling was found (p= 0.001, p= 0.001) on the flexural strength results, but thermocycling did not significantly affect the microhardness results (p= 0.078). The interaction factors were significant for both flexural strength and microhardness parameters (p= 0.001 and 0.002, respectively). Thermocycling decreased the flexural strength of the three IRCs tested significantly (p < 0.05), except for VITA Zeta (106.3 +/-9.1 to 97.2 +/-14 MPa) (p > 0.05) when compared with nonthermocycled groups. Microhardness results of only Sinfony were significantly affected by thermocycling (25.1 +/-2.1 to 31 +/-3.3 Kg/mm(2)). DC values ranged between 63% and 81%, and were not significantly different between the IRCs (p > 0.05). While a positive correlation was found between flexural strength and microhardness without (r = 0.309) and with thermocycling (r = 0.100) for VITA VMLC, negative correlations were found for Resilab under the same conditions (r =-0.190 and -0.305 AbstractPurpose: This study evaluated the degree of conversion (DC) of four indirect resin composites (IRCs) with various compositions processed in different polymerization units and investigated the effect of thermal aging on the flexural strength and Vicker's microhardness. Materials and Methods: Specimens were prepared from four IRC materials, namely Gr 1: Resilab (Wilcos); Gr2: Sinfony (3M ESPE); Gr3: VITA VMLC (VITA Zahnfabrik); Gr4: VITA Zeta (VITA Zahnfabrik) using special molds for flexural strength test (N = 80, n = 10 per group) (25 × 2 × 2 mm 3 , ISO 4049), for Vicker's microhardness test (N = 80, n = 10 per group) (5 × 4 mm 2 ) and for DC (N = 10) using FT-Raman Spectroscopy. For both fle...
The RS finish line produced MD values significantly lower than tilted and large chamfer, but large chamfer presented the lowest internal discrepancy values. Independent of the finish line type, internal discrepancy was the lowest in the axial region followed by radius and occlusal regions.
The CAD/CAM technology associated with rapid prototyping (RP) is already widely used in the fabrication of all-ceramic fixed prostheses and in the biomedical area; however, the use of this technology for the manufacture of metal frames for removable dentures is new. This work reports the results of a literature review conducted on the use of CAD/CAM and RP in the manufacture of removable partial dentures.
This study evaluated the effects of mechanical and thermal cycling on the flexural strength (ISO 9693) of three brands of ceramics fused to commercially pure titanium (cpTi). Metallic frameworks of 25×3×0.5 mm dimensions (N=84) were cast in cpTi, followed by 150-μm aluminum oxide airborne particle abrasion at a designated area of the frameworks (8×3 mm). Bonder and opaque ceramic were applied on the frameworks, and then the corresponding ceramic (Triceram, Super Porcelain Ti-22, Vita Titankeramik) was fired onto them (thickness: 1 mm). Half of the specimens from each ceramic-metal combination were randomly tested without aging (only water storage at 37ºC for 24 hours), while the other half were mechanically loaded (20,000 cycles under 10 N load, immersion in distilled water at 37℃) and thermocycled (3,000 cycles, between 5-55℃, dwell time of 13 seconds). After the flexural strength test, failure types were noted. Mechanical and thermal cycling decreased the mean flexural strength values significantly (p<0.05) for all the three ceramic-cpTi combinations tested when compared to the control group. In all the three groups, failure type was exclusively adhesive at the opaque ceramiccpTi interfacial zone with no presence of ceramic on the substrate surface except for a visible oxide layer.
This study evaluated the effect of mechanical cycling on the bond strength of zirconia posts to root dentin. Thirty single-rooted human teeth were transversally sectioned to a length of 16 mm. The canal preparation was performed with zirconia post system drills (CosmoPost, Ivoclar) to a depth of 12 mm. For post cementation, the canals were treated with total-etch, 3-steps All-Bond 2 (Bisco), and the posts were cemented with Duolink dual resin cement (Bisco). Three groups were formed (n = 10): G1 -control, no mechanical cycling; G2 -20,000 mechanical cycles; G3 -2,000,000 mechanical cycles. A 1.6-mm-thick punch induced loads of 50 N, at a 45° angle to the long axis of the specimens and at a frequency of 8 Hz directly on the posts. To evaluate the bond strengths, the specimens were sectioned perpendicular to the long axis of the teeth, generating 2-mm-thick slices, approximately (5 sections per teeth), which were subjected to the push-out test in a universal testing machine at a 1 mm/min crosshead speed. The push-out bond strength was affected by the mechanical cycling (1-way ANOVA, p = .0001). The results of the control group (7.7 ± 1.3 MPa) were statistically higher than those of G2 (3.9 ± 2.2 MPa) and G3 (3.3 ± 2.3 MPa). It was concluded that the mechanical cycling damaged the bond strength of zirconia posts to root dentin.
Objetivo: Este estudo propôs avaliar a microdureza de diferentes resinas compostas de uso direto (rcd) e indireto (rci).Materiais e Métodos: Com o auxílio de uma matriz metálica (diâmetro: 5,0mm; espessura: 2,0mm) foram confeccionadas 70 amostras, sendo (n=10) três resinas de uso direto: Gr1- Z250(3M ESPE/EUA), Gr2- W3D(Wilcos/Brasil) e Gr3- Esthetic X(Dentisply/EUA); e quatro de uso indireto: Gr4- Resilab Master (Wilcos/Brasil), Gr5- Vita VM LC (Vita Zahnfabrik/Alemanha), Gr6- Vita Zeta (Vita Zahnfabrik/Alemanha) e Gr7- Sinfony (3M ESPE/EUA). As amostras das rcd foram confeccionadas utilizando a técnica incremental, onde cada incremento de resina foi fotopolimerizado durante 40 segundos. Já as amostras da rci foram polimerizadas segundo recomendações dos fabricantes. Todos os espécimes foram armazenados em água destilada a 37ºC durante 24 horas. O teste de microdureza foi realizado em microdurômetro digital (Future-Tech, Modelo FM 700), com carga de 50 kgf por 15 segundos. Os dados obtidos (Kgf/mm2) foram analisados utilizando o teste não paramétrico de Kruskal-Wallis e o de comparação múltipla de Dunn (p<0.05). Resultados: As medidas resumo-numéricas de microdureza obtidas foram (mediana; média ± desvio padrão): Gr1 (100,12; 101,07± 5,99 Kgf/mm2), Gr2 (83,55; 84,20±5,07 Kgf/mm2), Gr3 (73,98; 73,95± 6,55 Kgf/mm2), Gr4 (52,50; 52,54± 5,9 Kgf/mm2), Gr5 (33,25; 34,36± 2,29 Kgf/mm2), Gr6 (29,60; 29.68± 1.52 Kgf/mm2), Gr7 (25,39; 25.13± 2.08 Kgf/mm2). Verificou-se que os valores de microdureza das rcd analisadas não diferiram estatisticamente entre si (p<0,05). O mesmo não se pode estabelecer para as resinas indiretas, pois a Sinfony diferiu da Resilab (p<0,05). Conclusão: Baseado nos resultados pôde-se concluir que apenas a resina composta direta Z250 apresentou valores de microdureza Vickers superior às demais resinas indiretas
O objetivo desta pesquisa foi estudar resistência à tração de cápsulas cimentadas a troqueis metálicos, com cimento fosfato de zinco, variando o alívio interno nas cápsulas e sulcos horizontais nas cápsulas e nos troqueis. Foram usinados em torno computadorizado (CNC), 288 cilindros, em aço inoxidável, simulando preparos para coroas totais (144) e respectivas coroas (144). Foram estabelecidas quarenta e oito condições experimentais, replicadas três vezes. Ajuste técnico de 2μm foi feito em todas as cápsulas para permitir assentamento. As cápsulas foram divididas em três grupos iguais em função do alívio. O grupo A não foi aliviado, os grupos B e C receberam 30μm e 60μm respectivamente. A quantidade de sulcos variou entre zero e três, tanto nas cápsulas como nos troqueis. A profundidade dos sulcos foi de 200μm. Os corpos-de-prova obtidos das cimentações com cimento fosfato de zinco foram submetidos a ensaio de tração em máquina universal de ensaios (Emic-Itaquaquecetuba-SP), no Departamento de Materiais e Tecnologia da Faculdade de Engenharia de Guaratinguetá, UNESP. Os resultados numéricos foram submetidos a tratamento estatístico (Análise de Variância e teste de Tukey). Os resultados mostraram diferença estatística significante (5%), individualmente e na interação das variáveis, alívio e quantidade de sulcos nas cápsulas. Não houve diferença estatística quanto à quantidade de sulcos nos troqueis. A análise dos resultados permitiu concluir que a resistência à tração: aumentou com o aumento do alívio e com a quantidade de sulcos nas cápsulas; permaneceu inalterada com os sulcos nos troqueis; parece ser limitada pelas variáveis estabelecidas para o troquel.
Minimizar discrepância de assentamento tem sido a razão de muitas pesquisas nos últimos tempos, visando melhorar a qualidade de adaptação das próteses dentárias. Entretanto, respeitados autores têm relatado resultados apresentando valores aparentemente incoerentes, isto é, melhor assentamento vertical de coroas totais após a cimentação, quando, devido à ausência de cimento interposto o inverso seria o esperado. Este fato levou- nos a desenvolver o presente trabalho. Assim, um dispositivo mecânico foi desenvolvido para padronizar e manter constante a pressão de assentamento durante todo o processo de mensuração (nas situações: sem cimento e após a cimentação). Para simular preparos coronários e coroas totais de segundos molares, foram utilizados modelos padrões e cápsulas metálicas como as propostas por Rocha et al6. O cimento utilizado foi o fosfato de zinco. As mensurações foram realizadas com o auxílio de um Metroscópio Carl Zeiss com resolução de 0,0001mm. Nossos resultados mostraram sempre valores maiores nas mensurações efetuadas após cimentação.
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