We consider dielectric measurements using a probe consisting of coaxial transmission line with an open-circuit end placed against the sample. For the 2.99 or 3.6 mm (OD) probes considered in this study, a simple lumped parameter model shows errors above 1 GHz that increase greatly with frequency. We evaluate an approximate model due originally to Marcuvitz, on the basis of measured probe impedances from 1 to 18 GHz with samples consisting of water, methanol, and dioxane-water mixtures. This model is more accurate than the lumped-parameter model, and is better suited for calibration of the automated network analyzer. Finally, we consider the errors introduced in dielectric measurements by the use of approximate models for the probe. The technique succeeds because of partial cancellation of errors in modeling the probe in ANAbased measurements.
An attempt was made to confirm previous reports of resonant-like dielectric absorption of plasmid DNA in aqueous solutions at 1-10 GHz. The dielectric properties of the sample were measured using an automatic network analyzer with two different techniques. One technique used an open-ended coaxial probe immersed in the sample; the other employed a coaxial transmission line. No resonances were observed that could be attributed to the sample; however, resonance-type artifacts were prominent in the probe measurements. The coaxial line technique appears to be less susceptible to such artifacts. We note two important sources of error in the calibration of the automatic network analyzer using the probe technique.
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