The dynamic fracture behavior of layered architectures is experimentally studied. Specifically, crack penetration, trapping, and branching at an interface are examined. A newly introduced optical technique called Digital Gradient Sensing (DGS) that quantifies elasto-optic effects due to a non-uniform state of stress is extended to perform full-field measurements during the fracture event using ultrahigh-speed photography. By exploiting the richness of two simultaneously measured orthogonal stress gradient fields, a modified approach for extracting stress intensity factors (SIFs) is implemented for propagating crack-tips under mixed-mode conditions. The method is first calibrated using a quasi-static experiment complemented by finite element simulations before implementing it for studying dynamic mixed-mode fracture mechanics of layered configurations. The layered systems considered consist of two PMMA sheets bonded using an acrylic adhesive with the interface oriented normally to the initial crack propagation direction. Interfaces are characterized as 'strong' and 'weak' by their crack initiation toughness. The dynamic fracture of monolithic PMMA sheet is also studied in the same configuration for comparison. The crack growth and fracture parameter histories of propagating cracks are evaluated. The interface is shown to drastically perturb crack growth behavior resulting in higher dissipation of fracture energy by exciting crack trapping, branching, and mixed-mode growth mechanisms.
Abstract. Highly transparent and tough graft-interpenetrating polymer networks (graft-IPNs) were synthesized using an elastomeric polyurethane phase (PU) and a highly stiff acrylate-base copolymer phase. The grafting points between the two networks were generated with the purpose of minimizing the phase separation process of the polymeric systems. In order to generate the grafting between the networks, an acrylic resin capable of undergoing both free radical and poly-addition polymerization was employed. The thermo-mechanical properties, fracture toughness properties as well as network and surface phase morphology of the graft-IPNs synthesized were evaluated in this work. Data obtained suggested that the minimization of the phase separation was achieved by the generation of crosslinking points between both networks. High transparency was obtained in all samples as an indication of the high level of interpenetration achieved. The relative high values obtained for the fracture toughness tests suggest that generating chemical crosslinks between networks is a good approach for increasing the fracture toughness of polymeric materials.
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