Thermolysis of [O~~(CO),~(dpprn)] (dppm = Ph2PCH2PPh2) in refluxing toluene affords a high yield of the unsaturated cluster [OS~(CO)~(H){ Ph2PCH2P(Ph)C6H4}] which has been characterised by X-ray crystallography, and which undergoes a facile reversible reaction with CO.
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