A facile green route has been employed for the synthesis of Zno and Ag-doped Zno using cannabis sativa as a reducing and stabilizing agent. the as-synthesized nanoparticles were characterized and tested for photocatalytic dye degradation and antimicrobial activity. the results suggested that nanoparticles have shown antimicrobial activity against different human pathogenic bacteria (Escherichia coli, Klebsiella pneumonia, MRSA, Pseudomonas aeruginosa, Salmonella typhi, Staphylococcus aureus) and fungal strains (Fusarium spp. and Rosellinia necatrix). Ag-doped nanoparticles comparatively have shown better removal congo red and methyl orange under visible light. Therefore, green synthesized nanoparticles could have beneficial applications in environmental science and biological field.
Herein, we report the synthesis of nanoparticles and doping of Cu-doped Co–Zn ferrites using the auto-combustion sol–gel synthesis technique. X-ray diffraction studies confirmed the single-phase structure of the samples with space group Fd3m and crystallite size in the range of 20.57–32.69 nm. Transmission electron microscopy micrographs and selected area electron diffraction patterns confirmed the polycrystalline nature of the ferrite nanoparticles. Energy-dispersive X-ray spectroscopy revealed the elemental composition in the absence of any impurity phases. Fourier-transform infrared studies showed the presence of two prominent peaks at approximately 420 cm−1 and 580 cm−1, showing metal–oxygen stretching and the formation of ferrite composite. X-ray photoelectron spectroscopy was employed to determine the oxidation states of Fe, Co, Zn, and Cu and O vacancies based on which cationic distributions at tetrahedral and octahedral sites are proposed. Dielectric spectroscopy showed that the samples exhibit Maxwell–Wagner interfacial polarization, which decreases as the frequency of the applied field increases. The dielectric loss of the samples was less than 1, confirming that the samples can be used for the fabrication of multilayer inductor chips. The ac conductivity of the samples increased with increasing doping and with frequency, and this has been explained by the hopping model. The hysteresis loops revealed that coercivity decreases slightly with doping, while the highest saturation magnetization of 55.61 emu/g was obtained when x = 0.1. The magnetic anisotropic constant was found to be less than 0.5, which suggests that the samples exhibit uniaxial anisotropy rather than cubic anisotropy. The squareness ratio indicates that the samples are useful in high-frequency applications.
Providing safe drinking water and clean water is becoming a more challenging task all around the world. Although some critical issues and limits remain unsolved, implementing ecologically sustainable nanomaterials (NMs) with unique features, e.g., highly efficient and selective, earth-abundance, renewability, low-cost manufacturing procedures, and stability, has become a priority. Carbon nanoparticles (NPs) offer tremendous promise in the sectors of energy and the environment. However, a series of far more ecologically friendly synthesis techniques based on natural, renewable, and less expensive waste resources must be explored. This will reduce greenhouse gas emissions and harmful material extraction and assist the development of green technologies. The progress achieved in the previous 10 years in the fabrication of novel carbon-based NMs utilizing waste materials as well as natural precursors is reviewed in this article. Research on carbon-based NPs and their production using naturally occurring precursors and waste materials focuses on this review research. Water treatment and purification using carbon NMs, notably for industrial and pharmaceutical wastes, has shown significant potential. Research in this area focuses on enhanced carbonaceous NMs, methods, and novel nano-sorbents for wastewater, drinking water, groundwater treatment, as well as ionic metal removal from aqueous environments. Discussed are the latest developments and challenges in environmentally friendly carbon and graphene quantum dot NMs.
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