Gaseous ozonation, an emerging technology, is applied to microbiological decontamination and to the degradation of residues and contaminants in wheat grains. However, due to its high oxidizing capacity, ozone may cause undesirable effects on the quality of grains or in their derivatives. This study aimed to evaluate the influence of ozone gas on wheat grain quality when exposed to different levels of ozone concentration, exposure time, and grain mass, using a full 2 3 factorial design. After the milling of ozonized grains, two fractions were evaluated: flour (A) and bran plus germ (B). In fraction A, the quality of the wheat flour was analyzed by both alveography and farinography. The flour extraction rate, falling number and gluten contents were also measured. The chemical and mineral profiles were determined in both fractions. A sensory evaluation, using the difference-from-control test, was applied to investigate the possible differences in aroma or in overall appearance of the flour obtained from the ozonized grains. The results showed that ozone concentration (60 mg/L) positively affected (p < 0.05) the toughness and the falling number of the flour. The other parameters of alveography, as well as farinography, gluten content, chemical composition, mineral, and sensory profiles were not affected (p > 0.05) by ozonation. This study demonstrated that gaseous ozonation, when applied under the conditions of 10 to 60 mg/L, from 2 to 5 h of exposure, grain mass from 2 to 5 kg, does not cause any negative impact on the wheat quality.
Mango
seeds from agro‐industry represents an environmental problem due to
the amounts of by‐products produced. Conversely, poly (lactic acid)
(PLA) is a potential green alternative to conventional plastics. The
goal of this study aimed to develop a biocomposite based on PLA and
mango’s by‐product for rigid packaging. Six biocomposites are
obtained by extrusion/injection processing using formulations with
PLA as a matrix and up to 20% by weight of mango seed’s
by‐products. The materials are characterized by chemical and
physical analysis; scanning
electron microscopy/energy dispersive X‐ray, X‐ray diffraction;
Fourier transform infrared spectroscopy (FTIR); thermal gravimetric
analysis/differential thermogravimetry; differential scanning
calorimetry (DSC), and mechanical analysis. FTIR bands and DSC transitions related to starch are higher in the kernel,
while more cellulose
bands are found in the integument. Kernel
presented thermal degradation in the biocomposites, the sample PLA+20
wt% kernel. For the other compositions, it is possible to observe
that they could keep their morphology. Significant improvements
in both mechanical and barrier properties are found in the formulation with 20 wt%
integument (up to 38% in elastic modulus). Therefore, this study
suggests that biocomposites
developed from PLA / Integument / Kernel have potential as a new biomaterial for rigid food packaging systems.
The processing to which a material is subjected can affect its physical or chemical structures, resulting in products with different hygroscopic behaviours. The present work studied the water adsorption properties of sorghum subjected to different types of processing: raw flour (produced by milling whole grain), extrudates (obtained using a double screw extruder) and extruded flour (obtained by milling the extrudates). The isotherms were obtained using an automated instrumental method. The tests were run in duplicate at 25 °C with relative humidity values ranging between 11 and 84%. The water adsorption data fitted the GAB model well, showing high coefficients of determination. The estimated water contents of the adsorption monolayer ranged from 5.3 to 6.9 g of water per 100 g of dry material. The sorption isotherms were affected by the type of processing, extrusion cooking resulting in products with less water in the monolayer (less hygroscopic). The milling process yielded high water contents in the monolayer, probably due to the breakdown of some polymer-polymer interactions, which exposed the binding sites. To ensure microbiological stability, the water contents in the materials should not exceed 6.9 g of water per 100 g of dry material for raw sorghum flour, 5.3 g of water per 100 g for sorghum extrudates and 6.7 g of water per 100 g for extruded sorghum flour.
Keywords: Extruded flour; Extrudates; Raw flour; Sorghum bicolor L.; Sorption isotherms.
ResumoO processamento ao qual um material é submetido pode afetar sua estrutura física ou química, resultando em produtos com diferentes comportamentos higroscópicos. No presente trabalho, objetivou-se estudar as propriedades de adsorção de água do sorgo em diferentes formas de processamento: farinha crua (produzida pela moagem de grãos inteiros), extrusados (produzidos em extrusora de duplo parafuso) e farinha extrusada (obtida pela moagem dos extrudados). As isotermas foram obtidas usando o método instrumental automatizado. Os testes foram realizados em duplicata, a 25 °C, com valores de umidade relativa variando entre 11 e 84%. Os dados de adsorção de água foram bem ajustados ao modelo de GAB, mostrando altos coeficientes de determinação. O teor estimado de água da monocamada variou de 5,3 a 6,9 g de água por 100 g de material seco. As isotermas de sorção foram afetadas pelo tipo de processamento, sendo que o cozimento por extrusão resultou em produtos com menor valor de monocamada (menos higroscópico). O processo de moagem produziu valores de monocamada elevados, provavelmente devidos à degradação de algumas interações polímero-polímero, que expuseram sítios de ligação. Para garantir a estabilidade microbiológica, o teor de água nos materiais não deve ser superior a 6,9 g de água por 100 g de material seco para a farinha crua de sorgo; 5,3 g de água por 100 g para os extrusados de sorgo, e 6,7 g de água por 100 g para a farinha extrusada.
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Sweet potato is one of the seven major staple crops in the world. Although most cream-fleshed sweet potatoes are produced locally, orange-fleshed sweet potato (OFSP) is an excellent source of beta-carotene and can be promoted to alleviate vitamin A deficiency. The aim of this study was to evaluate the retention of total carotenoids (TC) and all-trans-beta-carotene (ATBC) after processing and storage of cookies with different proportions of OFSP and margarine. Cookies formulated with 18 to 22.23 g/100 g of OFSP and 28.57 to 34.6 g/100 g of margarine were analyzed by spectrophotometry and high-performance liquid chromatography. The formulation containing the highest content of OFSP (22.23 g/100 g) and 32.84 g/100 g of margarine showed greater retention of TC and ATBC after processing. Among the other samples with the same proportion of OFSP, the one containing the highest margarine concentration (34.6 g/100 g) has shown a greater capacity to maintain TC and ATBC during storage (up to 56 days), demonstrating lipids important role in the preservation of these components.
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