Flat sheet polyethersulfone (PES) ultrafiltration membranes were fabricated by a dry/wet induced phase inversion process. Various ranges of ZnO concentrations (from 0 –5 wt. %) were utilized in conjunction with 16.5 and 2.5 wt. % of polyethersulfone and polyvinylpyrrolidone (PVP), respectively. The prepared membranes were characterized using scanning electron microscope (SEM), contact angle (CA), and flux/rejection performance. The modified membranes were tested on humic acid removal. The hydrophilicity of PES membrane was improved after addition of zinc oxide nanoparticles in the casting solution. Highest pure water flux was obtained at 5 wt.% ZnO nanoparticles. The modified membranes with 2.5 wt. % of zinc oxide exhibited higher humic acid flux and rejection.
The Nb2O5-Ni coating was processed using DC sputtering on structural steel and study characterization of composite coating SEM/EDS inspection indicated clearly perfect incorporation of Nb2O5 within the nickel rich. Increasing in surface roughness and decreasing in average diameters of particles were obtained for coated surface compared with uncoated surface from AFM analysis, in addition, microhardness test and thickness test showed that increasing of the hardness value to 163 HV for Nb2O5 - Ni composite coating compared to 132 HV for uncoated samples, the hardness for Ni coating also increasing to155 HV and the thickness for Nb2O5-Ni composite coatings increased significantly compared to uncoated samples.
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