To examine the feasibility of developing flame-retardant-textile coated fabric systems with electrospun polyamide/boric acid nanocomposites, fiber webs coated on cotton substrates were developed to impart-fire retardant properties. The morphology of the polyamide/ boric acid nanocomposite fibers was examined with scanning electron microscopy. The flame-retardant properties of coated fabric systems with different nanoparticle contents were assessed. The flame retardancy of the boric acid coated fabric systems was evaluated quantitatively with a flammability test apparatus fabricated on the basis of Consumer Product Safety Commission 16 Code of Federal Regulations part 1610 standard and also by thermogravimetric analysis. The 0.05 wt % boric acid nanocomposite fiber web coated on pure cotton fabric exhibited an increment in flame-spreading time of greater than 80%, and this indicated excellent fire protection. Also, the coated fabric systems with 0.05% boric acid nanocomposite fiber webs exhibited a distinct shift in the peak value in the thermal degradation profile and a 75% increase in char formation in the thermooxidative degradation profile, as indicated by the results of thermogravimetric analysis. The results show the feasibility of successfully imparting flame-retardant properties to cotton fabrics through the electrospinning of the polymer material with boric acid nanoparticles.
The effective dispersion of Graphene Nanosheet (GNS) as reinforcement was studied with various morphology of Copper (Cu) powder as matrix. High energy milling was used for modifying the morphology of the Cu powders. The Cu powder with Spherical and dentric shape was used in this study. Using high energy milling both the powders were milled for 8 h and 16 h respectively. The morphology of Cu powders was altered as flake shape upon milling. GNS (2 wt. %) was added as reinforcement uniformly with various morphology Cu powder used as matrix. The effect of size and shape of Cu as matrix on Cu/GNS composite properties was comprehensively studied. The Cu/GNS composite was prepared using powder metallurgy technique. Using the different shape and size of the Cu as matrix the interface of GNS has been studied. The hardness properties of Cu/GNS composite are evaluated. The effect of GNS interface in Cu particles has a significant influence on mechanical properties of composites. The hardness of Cu matrix composite has improved up to 20% compared to that of pure Cu. Thus morphology of Cu has the ability to improve the mechanical properties with GNS reinforcement.
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