A composite material, formed by the mixture of several elements, can be conveniently described by, from the way the radiation interacts with it, as if it were formed by a factitious element with an effective atomic number (Z ef ).This parameter is not constant with the energy, however, can be considered as an useful tool for characterization of biological tissues, tissue-equivalent materials and dosimeters. Several ways for the determination of Z ef were proposed by the literature, among them, are the attenuation methods which are based on the total cross section (derived form the mass attenuation coefficient (µ/ρ)) and the scatter methods which are based on the ratio between the Rayleigh and Compton differential cross sections. In this work, were study ways to obtain Z ef experimentally and theoretically by two methods (attenuation and scattering) to fill the gaps in the literature. In the attenuation method µ/ρ was used as interaction coefficient which, in the author's knowledge, it hasn't been used. For this purpose, experimental arrangements to determine the density (ρ) and the linear attenuation coefficient properly. In the attenuation method, the arrangements for determining µ/ρ allowed to determine it with differences smaller than 6% when compared with the literature and uncertainties of 3.8% for 59.54 keV and up to 7% in the range of 15 to 45 keV.It has also been found that the method is suitable for determining Z ef for energies of up to 60 keV, because above that energy, the uncertainties in Z ef increases (more than 10%). In the scattering method, the arrangement for determining R/C made it possible to obtain measurements of R/C with less than 10% difference with the literature and uncertainties of 7% and it was verified that the momentum transfer range between 1 Å −1 and 2 Å −1 is suitable for determining Z ef (uncertainties less than 3 % uncertainty).