“…These results showed that Zn-Al-NO 3 -LDH precursors started to transform to a ZnO phase at 200°C and higher. ZnAl 2 O 4 spinel is present in the samples Zn-Al-LDH-600°C, Zn-Al-LDH-800°C and Zn-Al-LDH-1000°C as observed by diffraction peaks at 2h = 31.4°, 36.9°, 44.8°, 49.1°, 55.7°, 59.4°and 65.3°, corresponding to the reflections from (2 2 0), (3 1 1), (4 0 0), (3 3 1), (4 2 2), (5 1 1) and (4 4 0) planes, respectively [19].…”