1999
DOI: 10.1143/jjap.38.l611
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X-Ray Rocking Curve Determination of Twist and Tilt Angles in GaN Films Grown by an Epitaxial-Lateral-Overgrowth Technique

Abstract: X-ray rocking curve measurements have been carried out in order to investigate the twisting and tilting in hydride vapor phase epitaxy (HVPE) and metalorganic vapor phase epitaxy (MOVPE) GaN films fabricated by an epitaxial lateral overgrowth (ELO) technique. The twist angle is directly determined by means of grazing incidence angle X-ray diffraction. It is found that these angles in both MOVPE and HVPE films are significantly reduced by the ELO technique especially for the twist angles. In… Show more

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Cited by 44 publications
(30 citation statements)
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“…3b. Recently, similar crystallographic tilts have been observed in lateral epitaxial overgrowths of GaN [11,12] and it has been suggested that the possible causes were factors like mask densification, etching and/or chemical instability which could lead to stresses sufficient to induce plastic deformation or a crystallographic tilt at the growth temperatures used, thereby relaxing the stresses in the layer [13]. In the growth of an AlN interlayer at a low temperature of 550 °C, a continuous amorphous layer would be expected to be formed; Akasaki et al [14] reported on the formation of an amorphous-like structure during lowtemperature AlN growth (600 °C).…”
Section: Methodssupporting
confidence: 69%
“…3b. Recently, similar crystallographic tilts have been observed in lateral epitaxial overgrowths of GaN [11,12] and it has been suggested that the possible causes were factors like mask densification, etching and/or chemical instability which could lead to stresses sufficient to induce plastic deformation or a crystallographic tilt at the growth temperatures used, thereby relaxing the stresses in the layer [13]. In the growth of an AlN interlayer at a low temperature of 550 °C, a continuous amorphous layer would be expected to be formed; Akasaki et al [14] reported on the formation of an amorphous-like structure during lowtemperature AlN growth (600 °C).…”
Section: Methodssupporting
confidence: 69%
“…Due to the weak scattering and extensive beam spill-off from the sample such measurements in the grazing incidence in-plane X-ray diffraction (GIIXD) geometry have been avoided in the laboratory and those reported have had poor signal and signal-to-noise ratio [6]. However, it has been shown recently that by use of a microfocus X-ray source and focusing optics, very high signals and good signal-to-noise can be obtained [7].…”
mentioning
confidence: 99%
“…This is principally due to the apparent growth of highly misorientated features within the epilayer as indicated by arrows B and C. These features correspond directly to highly misorientated features on the substrate (arrows B 0 and C 0 ). Additionally, it has previously been observed in the case of GaAs ELO on GaAs [14], that the ELO SiO 2 stripes can produce very high stresses in the underlying semiconductor. This can be observed as an array of vertically orientated stripes of the order of hundreds of microns long.…”
Section: Resultsmentioning
confidence: 93%