2014
DOI: 10.1186/s40543-014-0037-y
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Validation and measurement uncertainty evaluation of the ICP-OES method for the multi-elemental determination of essential and nonessential elements from medicinal plants and their aqueous extracts

Abstract: Background: The paper presents the development, validation, and evaluation of measurement uncertainty of a method for quantitative determination of essential and nonessential elements in medicinal plants and their aqueous extracts by using inductively coupled plasma optical emission spectrometry. Methods: The detailed validation of the analytical procedure and calculation of the measurement uncertainty budget allowed the recognition of the methods' critical points.

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Cited by 47 publications
(26 citation statements)
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“…Only [59] states that the analyzed plants originate from the spontaneous flora. One can only surmise that at least part of the analyzed samples in [42, 43, 46, 66] were harvested from the spontaneous flora, because the plants were purchased from the “local bazar or market” or were “plants growing in Turkey.”…”
Section: Discussionmentioning
confidence: 99%
“…Only [59] states that the analyzed plants originate from the spontaneous flora. One can only surmise that at least part of the analyzed samples in [42, 43, 46, 66] were harvested from the spontaneous flora, because the plants were purchased from the “local bazar or market” or were “plants growing in Turkey.”…”
Section: Discussionmentioning
confidence: 99%
“…The combined standard uncertainty was obtained by combining the uncertainties, according to the law of propagation of uncertainties. The final result was reported as expanded uncertainty, calculated by multiplying the standard uncertainty with the coverage factor (k=2), corresponding to a 95% confidence level [33]. The accuracy of measurements was assessed by determination of the studied elements in ERM-CC141 Loam Soil and IAEA-359 Cabbage CRMs.…”
Section: Methods Performance and Quality Controlmentioning
confidence: 99%
“…The contents of metals present in the garlic were determined using ICP-OES after the digestion of the samples with concentrated HNO3 and analyzed for Zn, Mg, Ca, P, Al and K in triplicate and the procedure as per method [12].…”
Section: Inductively Coupled Plasma Optical Emission Spectrometry (Icmentioning
confidence: 99%