Ultra-sensitive determination of cyanide in surface water by gas chromatography–tandem mass spectrometry after derivatization with 2-(dimethylamino)ethanethiol

Kang, Hye-In; Shin, Ho‐Sang

doi:10.1016/j.aca.2014.09.036

Cited by 11 publications

(5 citation statements)

References 48 publications

(76 reference statements)

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“… Mottier et al ( 2010 ) China 98.38 μg/cig. Xu et al ( 2006 ) Water Surface water Korea (Gum River) 1.01 ± 0.03 μg/L Kang and Shin ( 2014 ) – 0.77 mg/L Dadfarnia et al ( 2007 ) Brazil 25–50 μg/L Frizzarin and Rocha ( 2013 ) China – Wan et al ( 2015 ) Italy 5.11 μg/L Giuriati et al ( 2004 ) Drinking water USA (Sunnyvale) <LOD Christinson and Rohrer ( 2007 ) USA (San Jose) <LOD Sweden – Themelis et al ( 2009 ) Iran <LOD Absalan et al ( 2010 ) Tap water Iran 0.6 μg/L Abbasi et al ( 2010 ) Wastewater Petrochemical sludge 6.1–63.5 μg/L Dadfarnia et al ( 2007 ) Electroplating waste 0.04–1.2 μg/mL Hassan et al ( 2007 ) Petrochemical sludge 4600.2 μg/L Abbasi et al ( 2010 ) Gold cyanidation solution 540 mg/L Breuer et al ( 2011 ) Industrial wastewater – Noroozifar et al ( 2011 ) Soil Japan ...…”

Section: Cyanide Occurrence In the Environmentmentioning

confidence: 99%

Cyanides in the environment—analysis—problems and challenges

Jaszczak

Polkowska

Narkowicz

et al. 2017

Environ Sci Pollut Res

202

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Cyanide toxicity and their environmental impact are well known. Nevertheless, they are still used in the mining, galvanic and chemical industries. As a result of industrial activities, cyanides are released in various forms to all elements of the environment. In a natural environment, cyanide exists as cyanogenic glycosides in plants seeds. Too much consumption can cause unpleasant side effects. However, environmental tobacco smoke (ETS) is the most common source of cyanide. Live organisms have the ability to convert cyanide into less toxic compounds excreted with physiological fluids. The aim of this paper is to review the current state of knowledge on the behaviour of cyanide in the environment and its impact on the health and human life.

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Section: Cyanide Occurrence In the Environmentmentioning

confidence: 99%

Cyanides in the environment—analysis—problems and challenges

Jaszczak

Polkowska

Narkowicz

et al. 2017

Environ Sci Pollut Res

202

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“…Visually, the image of the population did not change over the survey days. Compared to the 100 and 500 µL samples, the population isolated in the 1000 µL sample was slightly larger from the start of the study, and at the time of the largest "jump" (around day [14][15], the size difference between the 100 and 500 µL and 1000 µL populations was as much as 10,000 particles.…”

Section: Variantmentioning

confidence: 83%

“…Pollution is caused by industrial sewage (electroplating plants, coking plants, gasworks, metal processing plants, etc.). These are very toxic compounds, and the sewage in which they are present should not be discharged into surface water reservoirs [14][15][16][17].…”

Section: Introductionmentioning

confidence: 99%

A Biological Method of Treating Surface Water Contaminated with Industrial Waste Leachate

Zamorska

Kiełb-Sotkiewicz

2021

Water

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The progressive chemicalization of all areas of everyday life and the development of the industry cause the appearance of various types of pollutants, both in groundwater and surface waters. Kalina Pond (Świętochłowice, Poland) is an example of a degraded water reservoir as a result of many years of activity, among others hard coal mines, storing metallurgical waste by zinc plants, and the activities of the Hajduki Chemical Plants from Chorzów. Inadequate securing of waste heaps resulted in the penetration of pollutants, i.e., phenol, petroleum compounds, PAHs, cyanides, and heavy metals. The aim of the research was to determine the suitability of biopreparations for the removal of pollutants. The research used a bacterial biopreparation from BioArcus, “DBC plus type R5”, to remove petroleum compounds and phenol. Then, in order to restore the microbiological balance, “ACS ODO-1” from the biopreparation was used. The research was carried out in laboratory conditions, using three variants: direct dosing of biopreparations, dosing of biopreparations previously activated by multiplication on the medium, and dosing of biopreparations into water after filtration on a diatomite bed. The optimal method of recultivating water from a reservoir was to filter this water through a diatomite bed and then dose the multiplied bacteria. After the filtration process, the obtained percentage of TOC reduction allowed for the rapid development of microorganisms from the biopreparation, despite the 100 times lower dose used. In addition, the application of lyophilized biopreparation to contaminated water resulted in a very fast biodegradation effect of pollutants, despite the high concentration of numerous toxic compounds.

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“…The linear working range of this system was between 40–1200 ng/mL with an LOD value of 20 ng/mL [38] . Another study reported the derivatization of for cyanide in surface water using 2‐dimethylamino)ethanethiol, coupled with a highly sensitive gas chromatography‐tandem mass spectrometry (GC‐MS/MS) system, which recorded an LOD value of 0.02 ng/mL [39] …”

Section: Resultsmentioning

confidence: 99%

“…[38] Another study reported the derivatization of for cyanide in surface water using 2-dimethylamino)ethanethiol, coupled with a highly sensitive gas chromatography-tandem mass spectrometry (GC-MS/MS) system, which recorded an LOD value of 0.02 ng/mL. [39] The method proposed in this study for the determination of cyanide does not require complicated derivatization steps, but involves a very simple, uncomplicated and practical process.…”

Section: Analytical Figures Of Meritmentioning

confidence: 96%

Colorimetric Sensor Based AgNPs for the Detection of Cyanide using UV‐Vis Spectrophotometry

Girgin,

Akbıyık,

Zaman

et al. 2023

ChemistrySelect

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Cyanide (CN−) is known to be a very harmful ion that may accumulate in the air, soil and water, and become a critical risk to organisms, even at trace levels. Hence, it is very critical to develop sensitive and accurate analytical methods for the determination of this anion. In this study, a highly sensitive and simple approach was developed for the quantitative determination of cyanide by UV‐Vis spectrophotometry with the aid of synthesized silver nanoparticles (AgNPs) solutions. AgNPs are promising probes frequently used in the determination of both organic and inorganic pollutants. The AgNPs were prepared by reducing silver nitrate (AgNO3) with sodium borohydride (NaBH4) in the presence of Triton X‐100 as a stabilizer. The UV‐Vis absorption spectra showed that the interaction between cyanide ions and AgNPs made significant decreases in the absorption peak of the surface plasmon resonance (SPR) band at 405 nm. The developed colorimetric sensor exhibited exceptional sensing towards cyanide ions with good linearity in the range of 0.5 and 3.5 mM. The limit of detection (LOD) and the limit of quantification (LOQ) were estimated as 0.09 and 0.29 mM, respectively. Moreover, the proposed colorimetric method was successfully applied to different water samples.

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Ultra-sensitive determination of cyanide in surface water by gas chromatography–tandem mass spectrometry after derivatization with 2-(dimethylamino)ethanethiol

Cited by 11 publications

References 48 publications

Cyanides in the environment—analysis—problems and challenges

Cyanides in the environment—analysis—problems and challenges

A Biological Method of Treating Surface Water Contaminated with Industrial Waste Leachate

Colorimetric Sensor Based AgNPs for the Detection of Cyanide using UV‐Vis Spectrophotometry

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