Über 3-Methyl-pyrrolizidin (2-Methyl-1-aza-bicyclo-[0,3,3]-octan)

Oreščanin-Majhofer, B.; Seiwerth, Rativoj

doi:10.1007/bf00913830

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-Methyl-and 3-hydroxymethylpyrrolizidines1

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1961

1970

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Cited by 5 publications

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“…employing PRELOG 'S (ISS) two-fold intramolecular alkylation. R = CHa) (350) with hydrobromic acid to yield the I.4.7-tribromoheptane (48. R = H) (377) and 4-(tetrahydrofuran-2-yl)-butan-2-ol (47.…”

Section: -Methyl-and 3-hydroxymethylpyrrolizidinesmentioning

confidence: 99%

“…350) reacted 2-acetylfuran (37) with ethyl bromoacetate under Reformatsky conditions to give the ethyl 3-hydroxy-3-furanyl-butyrate (38) which was dehydrated and reduced to the tetrahydrofuranylbutanol (39), treated with hydrobromic acid to I,4,7-tribromo-3-methylheptane (40) and hence to I-methylpyrrolizidine (41). 350) reacted 2-acetylfuran (37) with ethyl bromoacetate under Reformatsky conditions to give the ethyl 3-hydroxy-3-furanyl-butyrate (38) which was dehydrated and reduced to the tetrahydrofuranylbutanol (39), treated with hydrobromic acid to I,4,7-tribromo-3-methylheptane (40) and hence to I-methylpyrrolizidine (41).…”

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