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Triethyl [1‐14C]phosphonoacetate from [14C]carbon dioxide
Abstract: Lithiation of diethyl methylphosphonate (1) with n‐butyllithium followed by carbonation with [14C]carbon dioxide and esterification with diazoethane afforded high specific activity triethyl [1‐14C]phosphonoacetate (4) in 62% yield.
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1989
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