“…Thermolysis is a chemical process, by which a substance is decomposed into other substances by use of heat [4][5][6]. The catalytic thermolysis of desizing wastewater at 95 • C and autogenous pressure, in the presence of CuSO 4 catalyst, has proved its efficiency in reducing the COD by about 71.6% and color by about 82.7%, with substantial energy recovery in terms of solid residue [7]. Surfactants and dyes with high molecular weights are successfully removed by coagulation/flocculation processes followed by sedimentation, flotation and filtration.…”