It is noteworthy to mention that synthesizing the polyimide
aerogel
powder, which is carried out in this study, benefits from two advantages:
(i) the powder particles can be used for some specific applications
where the monolith is not suitable and (ii) there is a possibility
to investigate how a polyimide aerogel monolith can be made through
the polyimide powder to reduce its cost and cycle time. In this study,
two straightforward methods, wet gel grinding and emulsion, are introduced
to prepare polyimide aerogel powders using ambient pressure drying.
The microscopic properties of interest, including skeletal and porous
structures, microparticle size and assembly, combined with macroscopic
properties such as thermal stabilities and conductivities (0.039 W/m·K),
confirm that the fabricated microparticles with a size in the range
of 7–20 μm and porosity in the range of 65–85%
are thermally stable up to 500 °C.