In this paper, outgassing of the thin film vacuum package is analyzed by integrated MEMS (Microelectromechanical system) resonator and RBS (Rutherford backscattering spectroscopy). Outgassing behavior of different thin film packaging materials is studied by exodiffusion experiments. It is demonstrated that a high temperature pre anneal will greatly reduce the outgassing but can not eliminate it.
Thin film vacuum packagingThin film packaging technology is essential for miniaturization and high level integration of semiconductor components. It allows for the encapsulation of MEMS or ICs (Integrated Circuits) at the wafer level using micromachining technology before the standard IC packaging process [1].The typical steps for thin film packaging are illustrated in Fig. 1. The packaging process normally starts after the MEMS is fabricated and can be easily integrated into the back end of the MEMS process. The critical steps include sacrificial layer deposition, first thin film deposition, etching holes on the thin film, releasing the sacrificial layer through the etched holes, and sealing the package by another thin film layer. Fig. 1. A conceptual process flow of creating a thin film package around a MEMS device.The thin film package protects the free standing micro structures on the wafer and isolates the contamination in the environment. Compared with another wafer level packaging technique, the bonded package, it greatly reduces the size and cost of the package, and simplifies the process. Moreover, some thin film packages not only play a role in protection of the device, but also are a functional part of the whole systems [1]. For example, thin film vacuum packages are crucial parts of many MEMS to reduce air damping [2]. Normally, the vacuum inside the package is realized by sealing the packaging in a vacuum environment, for instance, by vacuum thin film deposition.The successful packaging of such MEMS by thin film technology relies on the long-term stability of the thin film material.
Outgassing of the thin film materialsVapor deposition technologies like PECVD (Plasma Enhanced Chemical Vapor Deposition) and LPCVD (Low Pressure Chemical Vapor Deposition) are typical ways to fabricate thin films [3]. Outgassing is one of the biggest concerns for the thin film vacuum package, since some gas molecules, like Hydrogen, may be incorporated inside the thin films during the deposition process [3] and may outgas under certain conditions. When outgassing happens, the freed gas will enter the inside of the thin film package and spoil the vacuum. This may happen after a long period of time or due to environmental changes such as thermal loading.Thermal loading is likely to happen in the MEMS process. For instance, a PECVD silicon nitride deposition with a thermal loading of about 300ºC to 450ºC may be used for the final anti scratch step for the wafers. Moreover, the temperature of standard IC packaging, which is often carried out after the thin film packaging, may reach several hundred degrees Celsius. The vacuum thin fil...