2003
DOI: 10.1016/s0272-8842(02)00195-5
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Thermal behaviour of alumina precursor obtained by the aluminium sulphate–urea reaction in boiling aqueous solution

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Cited by 35 publications
(16 citation statements)
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“…The homogeneous precipitation method in aqueous solution and some physicochemical properties of such oxide powders as Al 2 O 3 and ZnO were investigated in our previous work [17,18] -1 (BET) was obtained by the calcination of the precursors at 500°C for 2 hours. JEOL JEM-transmission electron microscopy (TEM ) images were taken to determine the morphology and dimension of the nanoparticles.…”
Section: Methodsmentioning
confidence: 99%
“…The homogeneous precipitation method in aqueous solution and some physicochemical properties of such oxide powders as Al 2 O 3 and ZnO were investigated in our previous work [17,18] -1 (BET) was obtained by the calcination of the precursors at 500°C for 2 hours. JEOL JEM-transmission electron microscopy (TEM ) images were taken to determine the morphology and dimension of the nanoparticles.…”
Section: Methodsmentioning
confidence: 99%
“…ZnO powders of different shapes, such as spindle-like, rod-like, ellipsoidal, spherical, and prismatic have been synthesized by the one or more of the methods mentioned above [16][17][18][19][20][21][22]. On the other hand, only a few methods were reported in the literature [23] to prepare ZnO powder having flake-like particles.…”
Section: Introductionmentioning
confidence: 99%
“…Comparing with the XRD patterns in Fig. 3a, it is testified that quartz had partly turned into cristobalite and that corundum (␣-Al 2 O 3 ) had formed from aluminum hydroxide coating through a series of phase changes [21,22]. From 1250 to 1300 • C, the diffraction peak intensities of cristo- balite and corundum become decreased and very weak at 1300 • C. This is because cristobalite, formed in flyash, gradually reacted with ␣-Al 2 O 3 coating to form secondary mullite.…”
Section: Effect Of Sintering Temperaturementioning
confidence: 93%