Thermal and X-Ray Crystallographic Structural Studies on (N,n-Dibencyl)-4-Nitrophenylsulfenamide

Brito, Iván; Restovic, A.; Pedrero, Samuel; Mancilla, Arlett; Vargas, Diego A.; León, Yasna; Ramírez, Eduardo; Arias, Mauricio; Brown, K.; Alvarez, Aldo; Arancibia, A. M. Muñoz; López-Rodríguez, Matías

doi:10.4067/s0717-97072003000300010

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Positive Ionization Mode: Ion Mobility Plasmagrams1

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Cited by 4 publications

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“…This effect can be eliminated working at low transfer line temperatures, but, depending on the thermal stability of the analyte it could not be enough to avoid fragmentation, as it is the case of the sulfonylureas [17].…”

Section: Positive Ionization Mode: Ion Mobility Plasmagramsmentioning

confidence: 99%

Spray nebulization for sample introduction in ion mobility spectrometry

Armenta

Gonzálvez

Blanco

2013

Analytica Chimica Acta

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Section: Positive Ionization Mode: Ion Mobility Plasmagramsmentioning

confidence: 99%

Spray nebulization for sample introduction in ion mobility spectrometry

Armenta

Gonzálvez

Blanco

2013

Analytica Chimica Acta

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“…These compounds contain trivalent nitrogen bonded to divalent sulfur. We have reported a series of sulfenamides prepared by the metal-assisted technique [27][28][29][30] . These sulfenamides have been of great interest to the chemical community because of their industrial applications, their usefulness as synthetic reagents, and ligands of compound coordination [31][32][33][34] .…”

Section: Introductionmentioning

confidence: 99%

SYNTHESIS AND CHARACTERIZATIONS OF Ag, Cu AND AgCu METALLIC NANOPARTICLES STABILIZED BY DIVALENT SULFUR LIGANDS

León

Brito

Cárdenas³

et al. 2009

J. Chil. Chem. Soc.

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The synthesis of Ag, Cu and Ag-Cu nanoparticles with divalent disulfur ligand by the Brust method were obtained. The metals were reduced by sodium borohydride and stabilized with 2,2'-dithioethanol (L1), N,N'-dithiophtalimide (L2) and triphenylmethanesulfenamide (L3). The nanoparticles were characterized by TEM, EDX, electron diffraction and FTIR. The stability of the colloids at room temperature was also measured. We can observe a high stability for the colloids dispersion with L3 ligand (>1 week by AgCu-L3, Ag-L3 and Cu-L3). We found TEM studies show a size distribution between 9.7 and 15.8 nm, depending on the ligand. Electron diffraction analysis for the metallic nanoparticles shows the presence of Ag 2 S, Ag, CuO and bimetallic compounds such as CuAgS. The active solids were obtained by solvent evaporation from the nanoparticles dispersed to 50 ºC. The FT-IR exhibit the presence of the ligand incorporated in the solid.

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Comparison of conventional and microwave-assisted synthesis of some new sulfenamides under free catalyst and ligand

Yakan

Kütük

2018

Monatsh Chem

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Thermal and X-Ray Crystallographic Structural Studies on (N,n-Dibencyl)-4-Nitrophenylsulfenamide

Cited by 4 publications

References 0 publications

Spray nebulization for sample introduction in ion mobility spectrometry

Spray nebulization for sample introduction in ion mobility spectrometry

SYNTHESIS AND CHARACTERIZATIONS OF Ag, Cu AND AgCu METALLIC NANOPARTICLES STABILIZED BY DIVALENT SULFUR LIGANDS

Comparison of conventional and microwave-assisted synthesis of some new sulfenamides under free catalyst and ligand

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