The Formation of a Solid from the Reaction SiCl4(g) + O2(g) = SiO2(s) + 2 Cl2(g)

Binnewies, Michael; Kornick, A.; Jerzembeck, Marion; Wilkening, Andreas; Quellhorst, Heike

doi:10.1002/9783527619924.ch18

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Mass Spectrometry and Chromatography1

Properties Of the Soot Porous Preforms1

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2010

2016

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“…In the case of the rearrangement of octa-[(n-heptyl) silsesquioxane], species up to n = 28 could be detected in the SEC traces (Falkenhagen et al 2003). Mass spectra showed that silsesquioxane structures with molecular weight up to approximately 5000 Da exist in a continuous distribution, confirming the results of theoretical calculations of Jug's group (Wichmann and Jug 1999;Binnewies and Jug 2000).…”

Section: Mass Spectrometry and Chromatographysupporting

confidence: 83%

Architecture of Silsesquioxanes

Dirè

Borovin

Ribot

2016

Handbook of Sol-Gel Science and Technology

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Section: Mass Spectrometry and Chromatographysupporting

confidence: 83%

Architecture of Silsesquioxanes

Dirè

Borovin

Ribot

2016

Handbook of Sol-Gel Science and Technology

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“…The flame temperature is, using our set of gas parameters, not high enough to initiate the hydrolyzation/oxidation of the SiCl 4 vapors. The flame was green on its whole length, which is interpreted as an incomplete reaction corresponding to the formation of intermediate chlorosiloxanes (Binnewies and Jug 2000;Wu and Greif 1996).…”

Section: Properties Of the Soot Porous Preformsmentioning

confidence: 99%

Experimental Study of SiO₂Soot Deposition using the Outside Vapor Deposition Method

Petit

Rouge

béclin³

et al. 2010

Aerosol Science and Technology

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The deposition of pure silica layers using the Outside Vapor Deposition method has been studied. The experimental study focuses on some fabrication parameters that have to be adjusted in order to work with a target temperature optimized for deposition of pure silica compatible with large volume deposition and post-treatments. It is experimentally shown that the optimized soot porous preforms are constituted by homogeneous silica spherical particles of 100 to 110 nm in diameter and have, in this case, densities approximately equal to 0.35 g.cm -3 .

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The Formation of a Solid from the Reaction SiCl₄(g) + O₂(g) = SiO₂(s) + 2 Cl₂(g)

Cited by 2 publications

References 3 publications

Architecture of Silsesquioxanes

Architecture of Silsesquioxanes

Experimental Study of SiO₂Soot Deposition using the Outside Vapor Deposition Method

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The Formation of a Solid from the Reaction SiCl4(g) + O2(g) = SiO2(s) + 2 Cl2(g)

Cited by 2 publications

References 3 publications

Architecture of Silsesquioxanes

Architecture of Silsesquioxanes

Experimental Study of SiO2Soot Deposition using the Outside Vapor Deposition Method

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The Formation of a Solid from the Reaction SiCl₄(g) + O₂(g) = SiO₂(s) + 2 Cl₂(g)

Experimental Study of SiO₂Soot Deposition using the Outside Vapor Deposition Method