“…By using the same procedure, reaction of 5 (1.00 g, 5.37 mmol) with N ‐(chloro(cyclohexyl)methylene)‐ N ‐methylmethanaminium chloride solution (prepared from a stirred mixture of N , N ‐dimethylcyclohexanecarboxamide (2.40 g, 15.5 mmol), phosphorus oxychloride (1.68 mL, 18.0 mmol), and dry chloroform (20 mL) at 0°C for 30 min) at reflux for 5 h gave 6c (1.20 g, 71%), purified by silica gel column chromatography (benzene) and recrystallized from ethyl acetate as colorless needles, mp 81–83°C; 1 H NMR (deuterochloroform): δ 1.19–2.20 (m, 10H, cyclohexyl‐H), 2.60–3.05 (m, 1H, H1′), 3.07 (t, 2H, J = 6.0 Hz, H5), 4.55 (t, 2H, J = 6.0 Hz, H6), 7.02–7.27 (m, 2H, H9 and 10), 7.46 (dd, 1H, J = 5.4, 2.7 Hz, H8), 8.04 (dd, 1H, J = 6.3, 2.7 Hz, H11); FABMS m / z 315 (MH + ), 317 (MH + + 2). Anal .…”