2012
DOI: 10.1007/s00542-012-1685-8
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The effect of atmospheric moisture on crack propagation in the interface between directly bonded silicon wafers

Abstract: Infra-red video sequences were taken of directly bonded silicon wafer pairs undergoing the razor blade crack length test for bond strength in a specially designed jig. A series of tests were carried out under controlled atmospheres of nitrogen at various relative humidities. Analysis of the video images showed that the crack continues to propagate rapidly for several minutes after the blade has stopped moving, and that the presence of moisture has a strong positive influence on the rate of crack propagation un… Show more

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Cited by 11 publications
(11 citation statements)
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References 15 publications
(19 reference statements)
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“…[3][4][5][6][7][8][9] In order to obtain the real bonding energy value, the measurement has to be done in anhydrous atmosphere. 8 Indeed as soon as siloxane bonds significantly appear at the bonding interface, during the blade insertion in humid atmosphere, the water corrodes them and the debonding length increases, reducing the apparent bonding energy.…”
Section: Direct Bonding Siloxane Bondsmentioning
confidence: 99%
See 2 more Smart Citations
“…[3][4][5][6][7][8][9] In order to obtain the real bonding energy value, the measurement has to be done in anhydrous atmosphere. 8 Indeed as soon as siloxane bonds significantly appear at the bonding interface, during the blade insertion in humid atmosphere, the water corrodes them and the debonding length increases, reducing the apparent bonding energy.…”
Section: Direct Bonding Siloxane Bondsmentioning
confidence: 99%
“…Masteika et al even succeeded in using all the WSC equations to recalculate the real direct bonding energy from the crack relaxation curves without having to use anhydrous atmosphere. 9 During direct bonding energy measurement using the DCB technique, the debonding length evolution and, maybe more significantly, its dependence on atmosphere humidity are then an indicator of siloxane bond presence at the bonding interface. This measurement allows us then to follow the classical silicon direct bonding reaction 1.…”
Section: Direct Bonding Siloxane Bondsmentioning
confidence: 99%
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“…al. 56 Both of these papers study the effect of ambient humidity on DCB testing. F. Fournel et al demonstrate the use of an anhydrous nitrogen atmosphere DCB testing apparatus that is able to produce highly repeatable results.…”
mentioning
confidence: 99%
“…However we initially found significant variation in bond strengths for identically processed bonded wafer pairs. Utilizing an optimized Maszara test 3 we were able to map the bond strength of a bonded wafer pair in 2 dimensions in order to determine the spatial extent and amplitude of any variation.…”
Section: Introductionmentioning
confidence: 99%