“…Anisotropic refinement was applied to all non-hydrogen atoms, and all of the hydrogen atoms were put at calculated positions. Crystal data for 3 at 153 K: MF ) Si 4C16H36, FW ) 340.80, triclinic a ) 9.7923 (8), b ) 14.5753(11), c ) 25.180(2) Å, R ) 89.960 (7), β ) 89.964 (7), γ ) 89.928 (7), V ) 3593.8(4) Å 3 , space group ) P-1 (No. 2), Z ) 6, dcalc ) 0.945 g cm -3 .…”