2016
DOI: 10.1016/j.microc.2016.06.008
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Technology issues of Byzantine glazed pottery from Corinth, Greece

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Cited by 27 publications
(18 citation statements)
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References 26 publications
(29 reference statements)
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“…; Palamara et al . ). That being said, other factors such as difference in the amount of lead oxides added to make the glaze and firing temperatures may also result in the observed difference in microstructure.…”
Section: Resultsmentioning
confidence: 97%
See 1 more Smart Citation
“…; Palamara et al . ). That being said, other factors such as difference in the amount of lead oxides added to make the glaze and firing temperatures may also result in the observed difference in microstructure.…”
Section: Resultsmentioning
confidence: 97%
“…Copper oxide (CuO) is the only type of colourant of these samples, with 1.13–4.17 wt% CuO being added to the alkali and alkali‐lead glaze to attain its characteristic turquoise hue (Palamara et al . , 143). An interesting observation here is that the glaze on the interior surface of JE10 has relatively low CuO concentration (< 1.0 wt%), but this glaze has an intense blue hue.…”
Section: Resultsmentioning
confidence: 99%
“…Non-destructive X-Ray Fluorescence (p-XRF) analysis was applied on all samples using a portable Bruker Tracer III SD set up, with a beam diameter of 3 mm; data quantification was made using S1PXRF software and a custom-built calibration curve, created in collaboration with the scientific personnel of Bruker. A detailed description of the calibration curve and the accuracy and precision achieved for the analysis of glass is provided elsewhere (Palamara, et al, 2016). In order to optimise the analytical range, two settings were used: (1) an unfiltered low-energy excitation mode (high voltage set at 15 kV and current of 24 μΑ, analyses carried out under vacuum) was used for the analysis of major and minor elements with an atomic number, Z, between 11 and 29; and (2) an Al/Ti filtered (0.012 inches Al plus 0.001 inches Ti) high-energy excitation mode (high voltage set at 40 kV and current of 12 μA) was used for the analysis of minor and trace elements with an atomic number Z > 29.…”
Section: Methodsmentioning
confidence: 99%
“…Each sample was measured at least three times. The accuracy and precision of the applied SEM/EDS setting has been described in detail elsewhere (Moropoulou, et al, 2016;Palamara, et al, 2016). Briefly, all major oxides in glass present high precision (error < 5%), with the exception of CaO which presents a deviation from the true value of approximately 10-15%.…”
Section: Methodsmentioning
confidence: 99%
“…The analysis was carried out with a portable Bruker Tracer III SD set up, with a beam diameter of 3 mm. The setting used was an Al/Ti filtered (0.012 inches Al plus 0.001 inches Ti) high-energy excitation mode (high voltage set at 40 kV and current of 12 μA) and the collection time of each measurement was 120 sec (Palamara, et al, 2016). The acquired data were only used qualitatively, due to the multi-layered structure of the samples, which was noted by the microscopic examination.…”
Section: Methodsmentioning
confidence: 99%