1978
DOI: 10.1002/jlcr.2580150148
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Synthesis of stereospecifically labelled [4-3H]cholesterol

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Cited by 12 publications
(5 citation statements)
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“…Furthermore Lockley et al. reported labeling of anilines with a homogeneous iridium catalyst . Even though there are already some examples published, there is still no simple and general method for the deuteration/tritiation of complex anilines.…”
Section: Methodsmentioning
confidence: 99%
“…Furthermore Lockley et al. reported labeling of anilines with a homogeneous iridium catalyst . Even though there are already some examples published, there is still no simple and general method for the deuteration/tritiation of complex anilines.…”
Section: Methodsmentioning
confidence: 99%
“…Location of the label in the [4 a-3H]and [4,B-3Hlcholesterol substrates used in this work (Lockley et al, 1978) indicated that 96 and 85%, respectively, of the 3H was in the expected positions. However, the latter value is probably an underestimate.…”
Section: Methodsmentioning
confidence: 64%
“…To investigate the possible role of a A4 compound cholesterol species were synthesized (Lockley et al, 1978). Incorporation of these cholesterol species into ecdysteroids would demonstrate whether either of the two C-4 hydrogen atoms of cholesterol is removed, irrespective of the stage at which it occurs.…”
mentioning
confidence: 99%
“…reported a frustrated Lewis pair‐catalyzed α‐deuteration of carbonyl compounds [13] . Also, late‐stage hydrogen isotope exchange, often mediated by an organometallic complex, has been a method of choice to incorporate a D or T [14, 15] …”
Section: Methodsmentioning
confidence: 99%