“…Compounds 2f-j were prepared by this method. Compound 2k has already been reported [29]. 2-(1,3-Benzothiazol-2-ylsulfanyl)-1-(4-methylphenyl) 2-(1,3-Benzothiazol-2-ylsulfanyl)-1-[1,1'- …”
Synthesis of novel 1,2,3-selena/thiadiazoles, linked to different benzo-1,3-heteroazole ring by sulfur has been reported. Structural features of the compounds have been analyzed by 1 H and 13 C NMR, mass and single crystal X-ray studies.
“…Compounds 2f-j were prepared by this method. Compound 2k has already been reported [29]. 2-(1,3-Benzothiazol-2-ylsulfanyl)-1-(4-methylphenyl) 2-(1,3-Benzothiazol-2-ylsulfanyl)-1-[1,1'- …”
Synthesis of novel 1,2,3-selena/thiadiazoles, linked to different benzo-1,3-heteroazole ring by sulfur has been reported. Structural features of the compounds have been analyzed by 1 H and 13 C NMR, mass and single crystal X-ray studies.
Electrochemical fluorination of 2-benzothiazolyl and 5-chloro-2-benzothiazolyl sulfides was successfully carried out using Et 4 NF‚3HF as a supporting electrolyte and fluoride ion source in dimethoxyethane to provide the corresponding R-monofluorinated sulfides in good yields. Fluorination took place selectively at the position R to the sulfur atom of the sulfides, and the heterocyclic moieties were not fluorinated at all.
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