volume 4, issue 1, P1-6 2013
DOI: 10.5155/eurjchem.4.1.1-6.718
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Abstract: KEYWORDS 2-Substituted 6-(5-oxo-1-phenylpyrrolidin-3-yl)pyrimidin-4(3H)-ones were synthesized in three steps from itaconic acid derivatives via cyclization with primary amines followed by Masamune-Claisen condensation, and cyclization of the newly formed β-keto esters with amidines. Preparation and/or isolation of β-keto esters with polar N-substituents failed, but the corresponding final products were obtained in a different way. 6-(1-(3-Hydroxypropyl)-5oxopyrrolidin-3-yl)-2-phenylpyrimidin-4(3H)-one was obt…

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