Abstract:6‐Methoxy‐3‐(2′‐thienyl)‐1,2‐benzisoxazole has been prepared simultaneously with 6‐methoxy‐2‐(2′‐thienyl)‐1,3‐benzoxazole. The spectral data of these new compounds have been discussed. Mass spectroscopy has proved to be a valid tool in the structural characterization of these isomers and 13C nmr spectrometry confirmed their structures.
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