“…Moreover, solvents, organic additives, and surfactants have important effects on the shape-and sizecontrolled synthesis of inorganic particles [23][24][25][26][27]. Although a few contributions have appeared on the synthesis of various morphological ZnSe, including hollow nanospheres/microspheres, nanowires, nanobelts and branched heterostructure, nanorods, flowerlike, and so forth [28][29][30][31][32][33][34][35][36][37][38][39], there have been few studies on fabrication of ZnSe spheres via surfactant-assisted solvothermal method. Herein, in this paper, we report a facile, convenient, and reliable solvothermal method to synthesis stilleite structure ZnSe microspheres.…”