Synthesis and crystal structure of bis(μ2-acetato-κ2
 O:O′)-di(ethanol)-bis{μ2-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ6
 O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C58H86Ni3N8O18

Ren, Zhi-An; Xiao, An; Liu, Ling-Zhi; Lan, Pengfei; Dong, Wen‐Kui

doi:10.1515/ncrs-2017-0388

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Zeitschrift Für Kristallographie - New Crystal Structures

2018

DOI: 10.1515/ncrs-2017-0388

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Synthesis and crystal structure of bis(μ₂-acetato-κ² O:O′)-di(ethanol)-bis{μ₂-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ⁶ O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C₅₈H₈₆Ni₃N₈O₁₈

Zhi-An Ren

An Xiao

Ling-Zhi Liu

et al.

Abstract: C58H86Ni3N8O18, triclinic, P1̅ (no. 2), a = 11.4561(8) Å, b = 13.1859(8) Å, c = 13.5063(11) Å, α = 109.620(7)°, β = 101.234(7)°, γ = 114.469(6)°, V = 1611.1(2) Å3, Z = 1, Rgt(F) = 0.0518, wRref(F2) = 0.1315, T = 173.69(10) K.

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The crystal structure of bis(μ₂-5-chloro-N-(2-methyl-1-oxidopropylidene)-2-oxidobenzohydrazonate-κ⁵ N,O,O′:N′,O′′)pentakis(pyridine-κ¹ N)tricopper(II), C₄₇H₄₅Cl₂N₉Cu₃O₆

Liguo

Zhang

Wang

et al. 2021

Zeitschrift Für Kristallographie - New Crystal Structures

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The crystal structure of bis(μ₂-5-chloro-N-(2-methyl-1-oxidopropylidene)-2-oxidobenzohydrazonate-κ⁵ N,O,O′:N′,O′′)pentakis(pyridine-κ¹ N)tricopper(II), C₄₇H₄₅Cl₂N₉Cu₃O₆

Liguo

Zhang

Wang

et al. 2021

Zeitschrift Für Kristallographie - New Crystal Structures

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show abstract

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Synthesis and crystal structure of bis(μ₂-acetato-κ² O:O′)-di(ethanol)-bis{μ₂-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ⁶ O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C₅₈H₈₆Ni₃N₈O₁₈

Abstract: C58H86Ni3N8O18, triclinic, P1̅ (no. 2), a = 11.4561(8) Å, b = 13.1859(8) Å, c = 13.5063(11) Å, α = 109.620(7)°, β = 101.234(7)°, γ = 114.469(6)°, V = 1611.1(2) Å3, Z = 1, Rgt(F) = 0.0518, wRref(F2) = 0.1315, T = 173.69(10) K.

Cited by 1 publication

References 19 publications

The crystal structure of bis(μ₂-5-chloro-N-(2-methyl-1-oxidopropylidene)-2-oxidobenzohydrazonate-κ⁵ N,O,O′:N′,O′′)pentakis(pyridine-κ¹ N)tricopper(II), C₄₇H₄₅Cl₂N₉Cu₃O₆

The crystal structure of bis(μ₂-5-chloro-N-(2-methyl-1-oxidopropylidene)-2-oxidobenzohydrazonate-κ⁵ N,O,O′:N′,O′′)pentakis(pyridine-κ¹ N)tricopper(II), C₄₇H₄₅Cl₂N₉Cu₃O₆

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Synthesis and crystal structure of bis(μ2-acetato-κ2 O:O′)-di(ethanol)-bis{μ2-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ6 O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C58H86Ni3N8O18

Abstract: C58H86Ni3N8O18, triclinic, P1̅ (no. 2), a = 11.4561(8) Å, b = 13.1859(8) Å, c = 13.5063(11) Å, α = 109.620(7)°, β = 101.234(7)°, γ = 114.469(6)°, V = 1611.1(2) Å3, Z = 1, Rgt(F) = 0.0518, wRref(F2) = 0.1315, T = 173.69(10) K.

Cited by 1 publication

References 19 publications

The crystal structure of bis(μ2-5-chloro-N-(2-methyl-1-oxidopropylidene)-2-oxidobenzohydrazonate-κ5 N,O,O′:N′,O′′)pentakis(pyridine-κ1 N)tricopper(II), C47H45Cl2N9Cu3O6

The crystal structure of bis(μ2-5-chloro-N-(2-methyl-1-oxidopropylidene)-2-oxidobenzohydrazonate-κ5 N,O,O′:N′,O′′)pentakis(pyridine-κ1 N)tricopper(II), C47H45Cl2N9Cu3O6

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Synthesis and crystal structure of bis(μ₂-acetato-κ² O:O′)-di(ethanol)-bis{μ₂-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ⁶ O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C₅₈H₈₆Ni₃N₈O₁₈

The crystal structure of bis(μ₂-5-chloro-N-(2-methyl-1-oxidopropylidene)-2-oxidobenzohydrazonate-κ⁵ N,O,O′:N′,O′′)pentakis(pyridine-κ¹ N)tricopper(II), C₄₇H₄₅Cl₂N₉Cu₃O₆

The crystal structure of bis(μ₂-5-chloro-N-(2-methyl-1-oxidopropylidene)-2-oxidobenzohydrazonate-κ⁵ N,O,O′:N′,O′′)pentakis(pyridine-κ¹ N)tricopper(II), C₄₇H₄₅Cl₂N₉Cu₃O₆